GCMS analysis summary, sample AD31377, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN1 5 02 \313 77 . D Vial: 23 Acq On : 16 Jan 2002 8:28 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 4.10 ug/1 877008 1,4-Dichlorobenzene-d4 11.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol/ 3-methyl- 102 C6H140 . 000077-74-7 36 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 Pentane,/3-methoxy- 102 C6H140 036839-67-5 9 Abundance Scan 262 (7.446 min): 31377.D (-) m/z 73.00 100.00% 73

5000 43

87 103 7.20 7.40 7.60 7.80 I, I 50 36— TI gm 55 67, । , ■ ■ j ■ < > * 1 > • 1 < 1 ■ i ' I ' 1 i ' ' ' 1 t 1,1 1 1 I 1 1 m/z 43.00 32.06% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63572: 3-Pentanol, 3-methyl- 73

5000 1 FT /l l 1 I " I- 1

55 7.20 7.40 7.60 7.80 45 87 m/z 45.05 12.19% : ' miz-> ________________ i 27 । 1 1 i • • ‘ 1 i • ■ ■ ‘ i ' ■ __10__ 20 .. 30 /amasl 40 50 60 +70 1 ‘ ■ i ■ 111 1*

80 90 100 110 Abundance 462932, Si 73 - TT ri 7.20 7.40 7.60 7.80 5000 m/z 41.05 11.76% 45 15 53 59 88 1 ' i ■ ‘ ■ i ■ ■ 1 ■ i • ■ ■ ■ i ■ 1 ■ ■ i ■ ■ ■ ■ i ■ ■ ' ' I 1 1 ‘ ' i ■ 1 1 1 i ‘ ■ i ■ ■ ' ' i ■ 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 30 #763: 1-Butanamine, 3-methyl- mPPmre --- 7.20 7.40 7.60 7.80 m/z 71.00 7.37% 5000

15 41 55 70 87 1**)i ■ ■ ''l1' I 1 I 1 ri 1 1 ' ' ' 1 1 1 1 ■ 1 i ' • 11 i ■ ■ ■ ■ I 1 ' ' 1 I 1 1 TIIunmmTTTTgT m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31377.D GCMS1126.M Mon Feb 04 15:07:58 2002 Page 1

NYC-WTC_000016143