GCMS calibration table with surrogate recovery data, Feb 16, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1502\1137.D Vial: 10 Acq On : 16 Feb 2002 12:12 am Operator: 209 GALOS Sample : gc/ms scan 1/16 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-1sopropoxy-1,1,1,7,7,7-hexam Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

37.49 0.46 ug/1 52411 Perylene-dl2 38.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Isopropoxy-1,1,1,7, 7,7-hexamethyl 576 C18H5207Si7 071579-69-6 37 2 1-Monolinoleoylglycerol trimethylsi 498 C27H54O4Si2 054284-45-6 36 3 Trisiloxane, 1,1,1, 5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 23 4 Mercaptoacetic acid, bis(trimethyls 2 36 C8H20O2SSi2 006398-62-5 Abundance 73.00 100.00% 23 73 Scan 3535 (37.493 min): 1137.D (-) m/ z 147 5000 221 281 355

m/z-> ri 1 1 hr 1 '1 r ' 4 50 100 1 150 200 250 253, 1 ■ i ■ ‘ 327 |........ 429 300 350 400 450 500 550 37.20 37.40 37.60 37.80 m/z 147.0.0' 68.27% Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3.5,5-tris(trim 73

5000 4 A AN ... MMRM 147 37'20 37.40 37.60 37.80 221 281 327 ... _ 415 519 581 -I1 1 _ ‘ i ■ ‘ 1 f i ' ' ■ ■ i "’ 1 1 1 1 1 1 1 ' I - 1

m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 73

207 37.20 37.40 37.60 37.80 5000 147 m/z 281.00 26.67% 34 103 281 395 482 ■ ■ । ■ 1 ■ ■ i ‘ ‘ । ■ ■ ■ • । ■ 1 i 1 1 1 1 i 1 1 1 1 i 1 1 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i m/z-> 50 100 150 200 250 300 400 350 450 500 ■r 1 ' i 1 1 550 M WW Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet T I ' ‘ ‘ 1 ' ' 73 147 37.20 37.40 37.60 37.80 281 m/z 207.00 18.07% 5000 Mawv UMwMa 369 T7l 1 1 1 T | l 1 207 249,11, r, aaaphasit 338 I....................................... m/z-> 50 100 150 200 250 300 350 400 450 500 550 37.20 37.40 37.60 3/80

1137.D GCMS0208.M Mon Mar 04 15:10:01 2002 Page 3

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