NYC-WTC_000035052
Laboratory report noting low pH and TurboVap contamination with recovery data for sample AD28691.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 24 pages
GCMS analysis comments for sample AD28677, Dec 2001
Machine-extracted title · confidence 100%Laboratory report noting low recovery rate and TurboVap contamination for sample AD28677.
NYC-WTC_000035171–000035194Folder label: “GCMS X 11/24/01 A 12/4/01”
Page image
OCR text
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC0401\28677.D Vial: 13 Acq On 5 Dec 2001 12:05 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 3-Isopropoxy-1,1,1,7,7,7-hexam Concentration Rank 16
R.T. EstConc Area Relative to ISTD R.T.
36.72 0.74 ug/1 127510 Perylene-dl2 37.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-1sopropoxy-1,1, $ 7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 2 Trisiloxane, 1,1/ ,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 10 3 3-Isopropoxy-1, 1, 1,5,5,5-hexamethyl 354 C12H3404Si4 072182-11-7 10 4 Silanamine, N-/t2,6-dimethyl-4- [ (tri 281 C14H27NOSi2 072088-09-6 10 Abundance Scan 3451 (36.723 min): 28677.D (-) m/z 73.00 100.00% 73
147 5000 221 281 355 ======== —50r + +7 36 TPT ... 191 । 253—432541401 . ............. 36.40 36.60 36.80 37.00 m/z 147.00 58.48%
1 m/z-> 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73
5000 TMrrT PrP44PT 147 36.40 36.60 36.80 37.00
221 281 m/z 221.05 44.81% 327 415 519 561 — ■
miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #52459 Trisiloxanc. : 1.1.5,5,5-hexamethyl-3,3-bis[(trimet 73 147 T’T TInt I"'' --AT 281 36.40 36.60 36.80 37.00 5000 m/z 281.00 20.99% 369 207 249 | 338 1 -r-rT-r-rT-r-pr-r-rT-p-r-T-ryT-r-'-rT-r^-i-T-rTT-r-r-r-r ■n—T-r—rrr- , < . i -nt m/z-? 50 100 150 200 250 300 350 400 450 500 550 Abundance #49645:3-lsopropoxy-1,i,1,5,5,5-hexamethyl-3-(trimethylsil 73 36.40 36.60 36.80 37.00 281 m/z 355.05 20.27% 5000 207 339
ms ' ' I ' ' 50 100 133 150 1771 1 200 249 1 । 250 300 350 400 450 500 550 4.....L ■ ■ i ■ ■ 1 1 I 36.40 36.60 36.80 37.00
28677.D GCMS1126.M Fri Dec 07 15:12:40 2001 Page 12
NYC-WTC_000035188
OCR can misread numbers and units. Confirm readings against the page image before using them.
NYC-WTC_000035188Source: NYC Law Department, mirrored locally
Related records
Browse subjects →Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
Same-box records
NYC-WTC_000035195
Laboratory report noting low pH and TurboVap contamination with recovery data for sample AD28689.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035072
Laboratory report noting TurboVap contamination and low recovery rate for sample AD28678.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035135
Laboratory report noting di-n-butylphthalate detection and low pH with recovery data for sample AD28694.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034971
Blank test results confirming no detectable contaminants above method detection limits for sample AD28662.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035153
Laboratory report noting TurboVap contamination and recovery data for sample AD28663.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034311
Laboratory report documenting GCMS analysis of sample AD28430 conducted on December 6, 2001.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035008
Laboratory report detailing GCMS scan results for sample AD28669, noting phthalate detection and recovery rates.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035089
Laboratory report noting TurboVap contamination with recovery data for sample AD28693.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Filed elsewhere
NYC-WTC_000088905
Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087274
Laboratory report documenting GC/MS analysis of sample AD22652 conducted on October 11, 2001, identifying unknown compounds.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗More like this page
Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Others also read
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000034946
Laboratory report detailing GCMS scan results for sample AD28650, noting phthalate detection and low pH.
Filed in the same folder
NYC-WTC_000034947
Document containing unreadable text or corrupted data from the Department of Environmental Protection archives.
Filed in the same folder
NYC-WTC_000034949
Form detailing Method 508 parameters and sample volume information for environmental testing procedures.
Filed in the same folder
NYC-WTC_000034954
Reference data sheet listing concentrations of volatile organic compounds detected in sample AD28662.
Filed in the same folder
NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
Filed in the same folder