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GC/MS analysis results for sample AD23500, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23500 conducted on October 19, 2001.

NYC-WTC_000088826–000088852

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088837
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NYC 9/11 Public Portal Document

Librar.y__Search_Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23500.D Vial: 8 Acq On : 16 Oct 2001 9:05 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L * * * * * * * ************************************************************** Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.51 ug/1 48602 1,4-Dichlorobenzene-d4 11.76

Hit# Of 5 intative ID MW MolForm CAS# Qual .

1 1,4-Dichl obenzene-d4 150 C6C12D4 003855-82-1.. 53 2 Benzene- ',2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 20: 3 Benzal A^yde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10\ 4 4-Ami -2-chlorobenzonitrile 152 C7H5C1N2 020925-27-3 9 ^bundance Scan 717 (11.625 min): 23500.D (-) m/z 149.90 100.00% 1ii0

5000- 115 52 78

I II I /-.-l-r ... . ....... 11.20 11.40 11.60 11.80 12.00 ... . m/z 151.90 67.83% ii/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593: 1,4-Dichlorobenzene-d4 1$0

115 78 11,20 11.40 11,60 11,80 12.00 52 m/z 115.00 35.42% 35 50 60 . ,,,11,.,°/,, 70 80 90 100 110 120 130 140 150 160 ^bundance —---- ---- #9592: Benzene-1,2,3,4-d4--5,6-dichloro- 1$0

115 11.20 11.40 11.60 11.80 12.00 ■ 5000 52 78 "mTz 78.05 20.97% A 35- 87 I I ' I ' ' ' ' I ' ' ' ' I ' ' I' ' ' ' I ' ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance „ #66892: Benzaldehyde, 2-hydroxy-3-methoxy-_________ „ „ 1$2 11.20-11-.40-11.60 11.80 12.00 Wz 52.00 17.86% 106 5000 53 • 81

92 122 136 I ' I ' ' ' ' I ' ' ' ' I ' T-|-T n-t- ' I ' ' ' ' I ' ' ' ' I TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23500.D NP091101.M Thu Oct 18 10:17:50 2001 Page 5,

NYC-WTC_000088837

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NYC-WTC_000088837Source: NYC Law Department, mirrored locally

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