GCMS analysis results for sample AE05897, March 29 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\5897.D Vial: 25 Acq On : 22 Mar 2002 12:56 pm Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Hexadecanoic acid Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

28.15 0.62 ug/1 242307 Phenanthrene-dl0 25.67

Hit# of 5 /Tentative ID MW MolForm CAS# Qual

1 Hexadecanofl-c acid 256 C16H32O2 000057-10-3 22 2 Isopropyl /Palmitate 298 C19H38O2 000142-91-6 22 3 7-(3,5-Dithethylisoxazol-4-yl)-triaz 256 C11H8N6O2 000000-00-0 14 4 Nonanoic acid 158 C9H18O2 000112-05-0 11 Abundance Scan 2517 (28.155 min): 5897.D (-) m/ z 4 3.05 43 102 60 5000 256 73 ...... / \ 129 239

rn/z-->____ 40 ■I. 60 80 100 120 140 160 180 200 220 240 ,________ 298 ' 'I ' ' ’'I''''I'' 260 280 300 27.80 28.00 28.20 28.40 m/z 102.05 68.11% Abundance #71608: Hexadecanoic acid 57 73 256

5000 - ■p’

129 27.80 28.00 28.20 28.40 m/z 60.05 58.90%

iTi/z-> 40 60 80 100_ 120 140 160 180 200 220 240 260 280_ 300 ■ Abundance #42488: isopropyl Pairnitate 102 I . .......Al...... . ■p 27.80 28.00 28.20 28.40 5000 60 m/ z 41.05 54.77% 73 129 85 157 257 rn/z->......... 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #35027; 7-(3,5-Dimethylisoxazol-4-yl)-triazolo[e]benzofuraz k ■p-T 43 27.80 28.00 28.20 28.40 m/z 57.00 43.30% 5000 256

159 239

m/z-> I 64 I I I I ' . . I I , 40 60 ■ 80 94 100 118 I "■pp 120 140 160 180 200 220 1 -rpr 240 260 280 300 .... . J,\...... 27.80 28.00 28.20 28.40

5897.D GCMS0308.M Mon Mar 25 14:27:21 2002 Page 2

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