GCMS analysis results, sample AE05234, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR3OO2\5234.D Vial: 45 Acq On : 31 Mar 2002 12:37 pm Operator: Sample : gc/ms scan 3/9 fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 Glaucic acid • Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

43.14 0.63 ug/1 39908 Perylene-dl2 37.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Glaucic acid 234 C15H22O2 087745-30-0 35 2 Cyclododecanecarbonitrile 193 C13H23N 069300-13-6 10 3 1,8-Nonadyene, 2,7-dimethyl-5-(1-me 192 C14H24 068702-20-5 10 JilQu^nolLhol, 4-(3-buten-l-ynyl)dec 233 C15H23NO» 037982-01-7 9 Abundance 5|5 8|1 Scan 4149 (43.138 min): 5234.D (-) 2- 5 m/z.21'5"715."Too . o'o% 41 93 107 133 67 233 119 149 5000 191 282

I ! T-p-T-r-r-p .IH.I.H, ........ 253 J_ 42.80 43.00 43.20 43.40 m/z 81.0.5 97.95% m/z-> 40 60 80 100 120 140 160 180__ 200 220 240 260 280 'Abundance ......... ...... .... .." #30729? Glaucic acid I 9(5 i 81 107 ^21 189 234 I 5000 133 177 42.80 43.00 43.20 43.40 219 m/z 55.10 94.12% 1m/2-> , I II I 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #21011: Cyclododecanscarboiiiinie 41 55 82 109 121 149 42.80 43.00 43.20 43.40 5000 135 . m/z 93.0,0 78.01% I 163

I 193 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 ‘Abundance #20858: 1,8-Nonadiene, 2.7-dimethyl-5-(1-methylethenyl)- 4 17 42.80 43.00 43.20 43.40 m/z 95.10 77.49% 93 5000 67 82 122 149

40 60 80 100 120 135

140 177 164 , J 192......... •160 180 200 220 240 ...................... 260 280 J i 42.80 43.00 43.20 43.40

5234.D GCMS0308.M Wed Apr 03 13:59:43 2002 Page 8

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