GCMS analysis results, sample AE04801, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2802\4801.D Vial: 13 Acq On : 28 Mar 2002 8:27 pm Operator: Sample : gc/ms scan 3/4 Inst ■ : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Nun±)er 4 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

37.37 0.84 ug/1 43017 Perylene-dl2 37.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual / 1 3,6-Dioxa-2,4y5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 32 2 3-IsopropoxWl,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 25 3 3-Trimethyl^ilyloxystearic acid, tr 444 C24H52O3Si2 000000-00-0 10 4 1,3-Benzodioxole, 5-[3-acetaminopro 221 C12H15NO3 000000-00-0 10 Abundance.............. ........................... Scan '3521 (37\372 min): 4801 .D (-j ....... ......... 7(3 147 221 5000 281 355 429 191 I , L 325, 37.00 37.20 37.40 37.60 37.80 ' I ' ' ' I ' ' ' ' I ' m/z 147.00 70.85% m/z-> 100 150 200 _____ 250 300 350 400 450 500 550 Abundance 147 2ii

73 ,A 5000 37.00 37.20 37.40 37.60 37.80 191 117 279 m/z 221.0,5 55.35% 250 ' 300 350 400 450 500 550 m/z-> 100 150 200 Abundance #50503: 3#aopropaxy-i, i .1.7.Cf-hexarnethyl-3.5,5-tris(trirr i 73

37.00 37.20 37.40 37.60 37.80 5000 147 m/z 355.05 33.90%

221 327 415 I I 519 561 m/z-> 100 150 200 250 300 350 400 450 500 550 Abundance #56734: 3-Trimethyisiiyloxyslearic acid, trimethyisiiyi est 7|3 37.00 37.20 37.40 37.60 37.80 m/z 281.05 28.06% 5000 147 233

313 429 189 1 339 387 [ I I I. , I m/z-> 100 150 200 250 300 350 400 450 500 550 37.00 37.20 37.40 37.60 37.80

4801.D GCMS0308.M Mon Apr 01 10:15:29 2002 Page 4

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