NYC-WTC_000058391
Analytical run record from April 2, 2002, documenting unknown compounds and surrogate recovery for sample AE04592.
1 shared topics · similarity 0.998
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GCMS analysis results for sample AE04411, April 2002
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of environmental sample AE04411 conducted on April 3, 2002.
NYC-WTC_000011877–000011892Folder label: “GCMS X 2/28/02 A 3/26/02”
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OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\l\DATA\MAR2502\4411.D Vial: 17 Acq On : 26 Mar 2002 1:59 am Operator: Sample : gc/ms scan 2/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
45.55 14.85 ug/1 1124460 Perylene-dl2 37.94
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 294 C10H300 i4 004342-25-0 47 2 Ethanedioic acid, bis (trimethyl si ly 234 C8H1804S:.2 018294-04-7 27 3 N-Benzhydrylidene-1- (2,4,6-trimethy 343 C24H25N0 089839-57-6 27 4 1,1,1,5,7,7,7/Heptamethyl-3f3-bis (t 444 C13H4005816 _ 038147-00-1 25 Scan 4412 (45.550 min): 4411.D (-) Abundance 73 /z 73.00 100.00% 147 221 5000 281 355 45.20 45.40 45.60 45.80 ' 429
m/z-> 44 “| ■•■■I 117 'I”uitjuihj— w91,a.442534RA744. 4011 m/z 147.00 PNdiu-lt 80.22% 40 60_80 100120 140160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane,2,2,4,4,5,5,7,7- ... ~ 147 221
73 5000 i - r. । r i 1 । । । । । 45.20 45.40 45.60 45.80 191 117 279 m/z 221.05 66.82%
mz-_ Abundance 40 60 80 100120140160 180200220 240 260 280 300 320 340 360 380400420 73 T T T I ■ * • * I • 147 45.20 45.40 45.60 45.80 5000 m/z 281.10 36.22% 45 117 190 219 m/z-> 40 60 80 100120140160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance #48514: N-Benzhydrylidene-1-(2,4,6-trimethylphenyl)ethylami 147 45.20 45.40 45.60 45.80 ‘ m/z 355.05 34.41% 5000
. ..... 1.165.197 312 343 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 420 ' . . । . . r . । . . . . t r 1 1 । । । । । । । ", m/z-> 45.20 45.40 45.60 45.80
4411.D GCMS0308.M Thu Mar 28 12:34:12 2002 Page 8
NYC-WTC_000011891
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NYC-WTC_000011891Source: NYC Law Department, mirrored locally
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