GCMS results sample AE08216, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1702\8216.D Vial: 27 Acq On : 18 Apr 2002 9:35 am Operator: Sample : gc/ms scan 4/8 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

37.32 0.45 ug/1 50766 Perylene-dl2 37.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7,' eptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 40 2 3-1sopropoxy 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 3 3,6-Dioxa-2, ■ ,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 16 4 Benzoic acid ,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 14 Abundance Scan 3515 (37.316 min): 8216. D (-) m/z 73.00 100.00% 73 147 221 5000 355 _) _ 281 429 ■ i ' ' ' ' i

m/z-> 1 44 ■ i 1 50 1 1 ' I ' ' ' '1 1 ' 100 II

150 193 , 2531 200 250 300 327 1, 350 401 - 400 450 500 550 37.00 37.20 37.40 37.60 m/z 146.95 71.30% Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73

147 5000 267 AAAAAy/ 1 ’■ r 1 1 1 ' I ' 1 1 1 I YCM 355 37.00 37.20 37.40 37.60 429 207 m/z 221.05 52.69% 45 1 1 1 I, ' ' i 1 ' ' ' i 1 I’I’I’’ m/z- > 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503:3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 A TT 37.00 37.20 37.40 37.60 5000 m/z 355.05 39.58% 147

■ 1 । 1 [ I I I i | I I । । | 221 I f i i | r 221 327 I r I | I I I I | I I I I | 415 I I I I | I I I । j 519 561 i 7 I I । r i

m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #41682: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5,7,7- 147 2.21 -AA I ' ' ' 1 I 37.00 37.20 37.40 37.60 m/z 281.00 36.83% 73 5000

117 191 279 AA—WW wass — n/z-> 50 100 150 200 tt 250 300 350 400 450 500 550 37.00 37.20 37.40 37.60

8216.D GCMS0412.M Thu Apr 18 14:13:22 2002 Page 2

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