GCMS results sample AE08216, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\APR1702\8216.D Vial: 27 Acq On : 18 Apr 2002 9:35 am Operator: Sample : gc/ms scan 4/8 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,1,1,5,7,7,7 -Heptamethyl-3,3- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

38.74 0.70 ug/1 79056 Perylene-dl2 37.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,1,1,5,7/7,7-Heptamethyl-3,3-bis(t 444 C13H40O5S16 038147-00-1 25 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 3 Amodiaquine 355 C20H22C1N3O 000086-42-0 9 4 Propanofc acid, 2-[(trimethylsilyl) 234 C9H2203Si2 017596-96-2 9 Abundance Scan 3670 (38.739 min): 8216.D (-) m/z73.00100.00% 73 |—— 147 5000 221 355 281 429 38.40 38.60 38.80 39.00 193 327 .. .......... ....... , ' ' i ' ■ 1 1 i ' 1 1 ' i ' ' —4 ' 1 i 11 T-TYT-r TTI TEBBnOTnT/fT ■ ■ । 1 1 ' ■ i ■ ■ ........ • hi m/z 147.00 58.19% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73

147 5000 267 355 38.40 38.60 38.80 39.00 429 207 m/z 221.05 45.01% 45 ..

A) 1 'i m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

38.40 :38.60 38.80 39.00 5000 m/z 355.05 25.56% 147

221 281 327 415 519 561 i lii i oi y 201 1 ' । ■ 1 1 । ' ' 1 ■ । 1 • • ■ i ■ r ■ ■ i • ■ । ■ i ■ ■ ■ • । • > ■ ■ । ■ i ■ ■■ • • i . ■ m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49807: Amodiaquine ..........I I I I I I I. I I I 1 1 1 1 1 1 I [ ' 1 1 58 38.40 38.60 38.80 39.00 282 m/z 207.00 23.61%

5000 355 ArMWonowy 1 218 253 ,...170 < ।k । l. r. | ri EUnl। i i i । - i-r । . m/z-> 50 100 150 200 250 300 350 400 450 500 550 38.40 38.60 38.80 39.00

8216.D GCMS0412.M Thu Apr 18 14:13:23 2002 Page 3

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