GCMS sample AE07067 analysis report with surrogate recovery, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\APR1802\7067.D Vial: 22 Acq On 19 Apr 2002 8:44 am Operator: Sample GC/MS SCAN 3/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Cyclohexanedione, 4-propyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 33.27 0.28 ug/1 49751 Chrysene-dl2 33.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Cyclohexanedione, 4-propyl- 154 C9H14O2 018456-81-0 38 2 1-Decene,/4-methyl- 154 C11H22 013151-29-6 32 3 Phenol, 3/ fluoro- 112 C6H5FO 000372-20-3 27 4 2-Cyclopenten-1-one, 2-hydroxy-3-me 112 C6H802 000080-71-7 27 Abundance ,7 Scan 3075 (33.272 min): 7067. D (-) m/z 112.10 100.00%

43 71 2 I 5000 83 \ 97 239 257 Lkt —44+r Li ii il Ji iIn । I । । IT । । I । । । । । । 129 . I. 3 1 [1 i i I-| i I I I j-! I I t i 1 < i | i 1281 "11471 i ) I I I I | I ! 33.00 33.20 33.40 33.60 m/ Z 57.00 96.32% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #10817:1,3-Cyclohexanedione, 4-propyl- 1 2

5000 55 70 84 33.00 33.20 33.40 33.60 m/z 71.10 72.50% 97 125 154 1 | | i | I | । । Cnn—-uu I I I I | iiii ] ! I —Tnnn l I I I | I T 1 1 i ■ ' m/z~> 100 120 140 160 180 200 220 240 260 280 Abundance #11046: 1 -Decene, 4-methyl- 57 71 A I 1 1 1 ' I ' ' 33.00 33.20 33.40 33.60 5000 112 m/z 70.10 70.06% 84 97 ।, 126....... 154........................................................ 1 1 i 1 l Tdt TT mlz~> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #2494: Phenol, 3-fluoro- 1 2 33.00 33.20 33.40 33.60 m/z 43.05 65 .48% 5000 83 64 37 49 J 95 ' ' ! 1 1 ■ ■ | । 1 1 l TT > [ I ' TT | I t r i । TT I | | I I ■ I | I I i i | i I I I [ I I I I | I I I T TT AA UL A m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 33.00 33.20 33.40 33.60

7067.D GCMS0419.M Mon Apr 22 08:33:12 2002 Page 1

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