GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC2 10130115.D Vial: 8 Acq On : 22 Dec 2001 1:41 pm Operator: 209 GALOS Sample : gc/ms scan 12 /13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Decanedioic acid, dibutyl este Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

29.29 0.54 ug/1 108538 Chrysene-dl2 33.01

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Decanedioic acid, dibutyl ester 314 C18H3404 000109-43-3 32 2 Cyclopentane, 1,1,3-trimethyl - 112 C8H16 004516-69-2 18 3 1-Hexene l 84 C6H12 000592-41-6 10 4 Cyclohexanone, 4-methyl-, thiosemic 185 C8H15N3S1 022397-22-4 10 Abundance Scan 2641 (29.286 mln): 30115.D (-) m/z 41.05 1 00.00% 41 241 56 185

5000 69 83 97 125 143 166 199 ll lllll ill III I । 110 1 29.00 29.20 29.40 29.60 It —4lu‘r Hlll— Ir * i * ' • ' i • ' * * I। * ,214 * * • । * * * > । • ■ m/z 241.15 84.98% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #73089: Decanedioic add, dibutyl ester 241 185 5000 56 T T TB." 98 29.00 29.20 29.40 29.60 125 143 199 73 84 166 m/z 56.00 77.71% • | i 214 | । ■ •' ■ । ‘ ■ ■ 1 1 ■ ■ ■ i ■ ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240

I Abundance #2676: Cyclopentane, 1,1,3-trimethyl- 55 41 • ■ i ■ • ■ ■ i ■ ■ 69 83 97 29.00 29.20 29.40 29.60 5000 77.53% 27

r 1 112 । ■'' ■ । ■ mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #62755:1-Hexene 411 56 29'00 29.20 29.40 29.60 27 m/z 55.00 75.87% 5000 84 69 1 । ■ • । ■ I* । I, AAALAALYyAA m/z-> 20 40 I * ‘ 60 ‘ I 80 100 120 140 160 180 200 220 240 29.00 29.20 29.40 29.60

30115.D GCMS1126.M Wed Jan 02 10:13:23 2002 Page 3

NYC-WTC_000019079