GCMS sample analysis results, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\30115.D Vial: 8 Acq On : 22 Dec 2001 1:41 pm Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.69 7.04 ug/1 2016220 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, /-hydroxy-4-methyl- 116 C6H1202 000123-42-2 83 2 CH2=CHCH2C (0) OCH3 100 C5H802 003724-55-8 10 3 5-Hexen-2-one 98 C6H10O 000109-49-9 9 4 3-Hydroxy/2-pentanone 102 C5H10O2 003142-66-3 9 Abundance Scan 289 (7.694 min): 30115.D (-) m/z 42.95 100.00% 43

5000 59

101 ■ > I • * • • i * > • » i > • ■ • । ■

miz-> Abundance 1 1 I ' 1 ' 1 I 1 1 ' 1 I 1 1 1 ' r' 11100/8 I ■ ■ 1 ■ I ■ ■ ■ 1 i 1 ' 1 1 i 1 10 20 30 ........... 38,11 40 , 48 53., . 66 50 60 70 75 80 83 88 90 #64274: 2-Pentanone, 4-hydroxy-4-methyl- a 110 m/z 59.1 100 7.40 7.60 7.80 8.00 48.27%

43

5000 59 7.40 7.60 ' 7.80 8.00 m/z 101.05 18.31% 27 101 83 m/z-> 11/22% 10 20 30 40 50 l i • • • > i • • • • i •' • • • j । 60 70 80 90 1 100 ■ । 1 110 Abundance #1448: CH2=CHCH2C(O)OCH3 43 ■ ■ । • i ■ ■ ■ ‘ 18a ।. j.. 7.40 7.60 7.80 8.00 5000 m/z 58.05 15.97%

58 ■ ■ i ■ • ■ ' i ■ ■ ■ ■ i ■ ■ ■ 38 ■ i ■ ■ ' ' i • ' ■ ■ i ■ ■ 72..........100........ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one TIIemTTuo 43 7.40 7.60 7.80 8.00 m/z 41.05 7.10% 5000

27 55 15 50 I 83 98 m/z-> I 1 i | ! ii ! 1$ > F j i r 10 20 30 38,+ 40 1 ■ ■ i 50 1 ■ i ■ ‘ 60 ‘ i 1 ■ ■ ' i • • • ■ i 1 ' • 1 i ■ ■ ■ • i • 70 80 90 100 110 1 1s W'r । j n j-j Ig" 7.40 7.60 7.80 8.00

30115.D GCMS1126.M Wed Jan 02 10:13:12 2002 Page 2

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