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GC/MS analysis report, sample AD23722, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23722 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089247–000089258

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089256
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23722.D Vial: 18 Acq On : 16 Oct 2001 4:48 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 7.77 0.59 ug/1 53106 1,4-Dichlorobenzene-d4 11.76

Hit# of 5 Tent^ ve ID MW MolForm CAS# Qual

1 2-Pentanone, -hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Butane 58 C4H10 000106-97-8 9 3 5-Hexen- -one 98 C6H10O 000109-49-9 9 4 2-Pent. ol, 2,3-dimethy1- 116 C7H16O 004911-70-0 9 fiibundance Scan 297 (7.766 min): 23722.D (-) m/z 42.95 100.00% 4b

■n^-> 5000

' I ' ' ’ ■ I ■ ■ • • I ■ • ■

10 20 30 40 /l

50 60 59

70 I I ‘ 83 ' I '' ' ' I 80 90 101

100 740 m/z 7.60 59.05 L 7.80 8.00 51.39% 8.20

Abundance #3245; 2-Pentanone, 4-hydroxy-4-methyl- 4b

5000 59 7.40 7.60 7.80 8.00 8.20 m/z 100.95 19.58% 31 I I

TiZz-> 10 20 30 4p 5p 6p 70 8p 90 ip0 Abundance #99; Butane -43 ............... ............................... 7.40' '7.60' 7.80 's.to' 8.20 5000 29 m/z 58.05 16.80%

15 58 ------------ ' ' I nfe-> 10 20 30 40 50 60 70 80 90 100 Abundance #63205:5-Hexen-2-one A .4h_---------- ----------- I * ' ' 'J 'T 7.40 7.60 7.80‘8.00^--8.20 m/z 4 0.95 8.83%

5000

55 15 V 50. I_________ 83_ 98 ' I ' ‘ I I ' I ' ' ‘ ' I ' ' ' ' I ' 38 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' 1 ' ' ' ' I ■ ' ■ I I ' ' ' I I Tlfe-> 10 20 30 40 50 60 70 80 90 100 7.40 7.60 7.80 8.00 8.20

23722.D NP091101.M Tue Oct 16 15:17:46 2001 Page 2

NYC-WTC_000089256

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NYC-WTC_000089256Source: NYC Law Department, mirrored locally

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