GCMS analysis results for sample AD25873, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2001\25873.D Vial: 5 Acq On : 20 Nov 2001 4:30 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.73 4.50 ug/1 887158 l,4-Dichlorobenzene-d4 11.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, A-hydroxy-4-methyl- 116 C6H1202 000123-42-2 50 2 Acetone / 58 C3H60 000067-64-1 10 3 Butane, 1-ethoxy- 102 C6H140 000628-81-9 9 4 5-Hexen-2-one 98 C6H10O _ 000109-49-9 9 Abundance Scan 293 (7.731 min): 25873.D (-) m/z 43.05 100.00% 43 59 5000 101 —*1011011—9100— __ 7.40 7.60 7.80 8.00 • ■ i ■ • • • i ■ ■ -34 — . T 53 , 69 77 83 11 । i-i l । m/z 59.05 51.38% miz-? 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 ’1 i 1 - । ( i . p . . -yi . i । । 59 7.40 7.60 7.80 8.00 m/z 100.95 22.15% 15 31 . 101 _ _I । । 83 । * ■ i ■ ■ • ‘I 11 1 1 1 1 TT 1 ■ ■ l ■ opnmpuuauItIu—tr m/z-? ___ IP____ 20 30 40 50 60 70 80 90 100 110 Abundance #62322. Acctone 43 ■ ■ i • • • • । • ■ • • | ■ 11it i ' | 7.40 7.60 7.80 8.00

L 5000 m/z 58.05 17.25% 58 27 Tgaaa/n/Bn—n————g/0—k—8—B-—B—————T-T—00T miz-> _.. 10___ 20__ 30____40 50 60____70 80 90__ 100 110 Abundance #63550: Butane, 1 -ethoxy- r ‘ i ■ ■ 1 ■ i ' । 1 ■ i ■ • ' • • • | 59 7.40 7.60 7.80 8.00_____ 31 m/z 41.05 7.40%

5000-

45 73 — - —......... — I ' 1 | 87 102 1 I ■ ■ • 1 i ■ • ■ ■ i ■ 1 1 ‘ 1 I ' ' '' 1 I 1 1 1 ' I 1 TTTTTTITEPF m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

25873.D NP103001.M Tue Dec 11 09:20:26 2001 Page 2

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