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GCMS analysis results for sample AD24292, Nov 5 2001

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Laboratory report documenting GCMS analysis of sample AD24292 conducted on November 5, 2001, noting unknown compounds.

NYC-WTC_000068185–000068197

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3101\24291.D Vial: 7 Acq On : 31 Oct 2001 9:58 pm Operator: 209 GALOS San^le : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *****************************************************************'**** Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 0.87 ug/1 119035 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4;>hydroxy-4-methyl- 116 C6H12O2 000123-42-2 56 2 3-Hydroxy-3^>irt^hyl-2-butanone 102 C5H10O2 000115-22-0 17 3 Acetone 58 C3H6O 000067-64-1 10 4 Oxirangy [ (1-methylethoxy) methyl] - 116 C6H12O2 004016-14-2 9 Wjundance Scan 289 (7.695 min): 24291 .D (-) m/z 42.95 100.00% 40

59 5000 101 7.40 7.60 7.80 8.00 83 m/z 59705^ 51.25% TTT+TT-TTrrr nZz-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

■ , ..................... .............................................. 5000 59 7.40 7.60 7,80 8.00 m/z 100.95 22.16% 27 101 I" I ‘ J I" " I 83 TiZz-> 15 20 25 30 35 40 45 50 55 K) 65 70 75 80 85 90 95 100 105 Wjundance #1697:3-Hydroxy-3-methyl-2-butanone 5b • > 1 I ■ 7.40 7.60 7.80 8.00 5000 m/z 58.05 17.35% 43 31

69 87 TTp-h+r TTy 1 • *" I infe-> 15 20253035404550556065 70 75 80859095 100105 ... Abundance Acetone 413 "7.^' 7.60 7.80 8.00 m/z 41.05 6.80% 5000 58 27 ‘ ' I''" |l' 'I I'"' I “' H'' i| I “I) >>"11 • ' 1" "I'"' I" " I'"' I" " I'"' 1" " I" " I'"' I"

Tlfe-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 7.^' ’7.60' 7.ot’ 8.66

24291.D NP103001.M Fri Nov 02 12:03:35 2001 Page 2

NYC-WTC_000068194

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NYC-WTC_000068194Source: NYC Law Department, mirrored locally

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