GCMS surrogate recovery results, sample AE00164, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB14O2\164.D Vial: 35 Acq On : 15 Feb 2002 12:12 pm Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.31 0.57 ug/1 67986 1,4-Dichlorobenzene-d4 12.34

Hit# Of 5 Tentative ID MW MolForm CAS# Qual ------------- 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 50 2 1-Propen-2-01, acetate 100 C5H802 000108-22-5 10 3 CH2=CHCH2CAO)OCH3 100 C5H802 003724-55-8 10 4 2,3-Butanedione, monooxime 101 C4H7NO2 000057-71-6 9 Abundance Scan 356 (8 311 min): 164.D (-) m/z.43.05100.00% 43

5000 59

101 1 1 ■ i 1 8.00 N8.20 I ' ' 1 r I 8.40__ 8.60_____ 51 — 83 .................. 39,11 1 ' ' I'1 1 1 1 1-mi i ''1 0 Hr— m/ z 59.05 45.38% m/z-> 10 20 30 40 50 60 70 80 90 100 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 .)1 1m . . । .... । 59 8.00 8.20 8.40 8.60 m/ z 58.05 15.32% 15 31 101 83 1 ■ ' i ' ' ' ■ i ' ■ 1 *1 111 । । 1 I i ‘ । । । I 1 1 i ' 1 ' ' i ‘ r ' 1 i 1'' 1 ' 1 1 1 ' 1 . ......... miz-? 10 20 30 40 50 60 70 80 90 100 Abundance 43 ' 1 1 I ' ' ' 1 1 ' f 1 1 1 1 1 1 ‘ I ' ' ' ' I 8.00 8.20 8.40 8.60 5000 m/z 101.05 14.11% 15 58 27 38 72 100 m/z->_ Abundance ■ ' i ■ 1 10 ■ ■ i ' 20 1 1 1 I 30 ' 1 i 1 40 1 ' ■ i 50 60 ' ■ ' 1 i ' 70 #1448: CH2=CHCH2C(O)OCH3 80 1 1 ■ i ■ ' 1 ' i 1 ‘ ' 1 i ■ ' ' 90 1 100 i '

■ ■ l • • ■ ■ I 43 8.00 8.20 8.40 8.60 m/z 41.05 7.47% 5000

58 72 100 ......................... 381 ■ ■ j > ■ ■ ■ i • > • ■ I > । । >' I • i PII—mT m/z-> 10 20 30 40 50 60 70 80 90 100 8.00 8.20 8.40 8.60

164.D GCMS0208.M Fri Feb 15 14:01:51 2002 Page 1

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