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GCMS analysis results for sample AE02647, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02647.

NYC-WTC_000005448–000005462

Folder label: “GCMS X 2/5/02 A 3/7/02

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Scanned page image, NYC-WTC_000005455
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0702\2647.D Vial: 20 Acq On 8 Mar 2002 8:25 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

8.19 0.38 ug/1 46379 1,4-Dichlorobenzene-d4 12.30

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol/ 3-methyl- 102 C6H140 000077-74-7 9 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 5 3 N-Ethylformamide 73 C3H7NO 000627-45-2 5 4 1,3-Dioxolane, Abundance / (1-methylpropyl) 2-Scan 343 (8.191 min): 2647.D (-) - 130 C7H14O2 014447-25-7 4 .. m/z 73.00 100.00%; 7b

5000 43

87 103 7.80_ 8.00 8.20 V 8.40 8.60

m/z->......... 10...... 20 30 p57 40 50 ..... 60 1170 80 90 100 110 m/z ‘ 43.05 32.15% Abundance #63573: 3-Pentanoi, 3-methyi- 73

5000 ..... / h...... 7.80 8.00 8.20 8.40 8.60 55 m/z 40.95 11.77% 45 87 27 39 1 ' i ' ' IIIIIIIIII m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 30 1........ I, ' i ' ' ' ' i ■ ' ' ■ i ' ' 7.80 8.00 8.20 8.40 8.60 5000 m/ z 45.05 11.24%

15 ' 41 55 70 87 III*/nn*I*I*IIIIIIIIII*NII1II*IIIIIII**IIIII m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 7.80 8.00 8.20 8.40 8.60 73 m/z 71.00 7.03% 5000 44 58 15 ■ ■ i > ■ ■ ■ । > ■ —I i 1 ‘ I ' ' ' ' । ' ' I........................I ' I | ' ! ) ' | I m/z-> 10 20 30 40 50 60 70 80 90 100 110 i 7.80 8.00 8.20 8.40 8.60

2647.D GCMS0208.M Wed Mar 13 14:58:13 2002 Page 1

NYC-WTC_000005455

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NYC-WTC_000005455Source: NYC Law Department, mirrored locally

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