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GC/MS calibration data for sample 30643, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018445–000018469

Folder label: “GCMS X 12/18/01 A 12/30/01

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NYC 9/11 Public Portal Document

Library -Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30643 .D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C: \HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T.

7.75 0.36 ug/1 178693 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 - Propanone, 1,1,1- trichloro- 160 C3H3C130 000918-00-3 38 2 2-Propanone, 1/1-dichloro- 126 C3H4C120 000513-88-2 12 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 4 2-Acetylthiazole ________________ 127 C5H5NOS 024295-03-2 7 Abundance Scan 295 (7.752 min): 30643.D (-) m/z 42.95 100.00% 43

5000 I 1 j f i"» । । » » » i j“ r j -t I । » » । 1 । » 7.40 7.60 7.80 8.00 _________ 36, .49 93 70 82. %103 *’I**’*1+*’’I’*1- i1 I 1+’ I I ’71+t I : ] I ... | 114 i I i i 84 11917 . ’44 I 1 m/z 124.95 10.22% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #12247:2-Propanone, 1,1,1-trichloro- 43 %

5000 ■ ' i ■ ■ ■ • i ■ ■ ■ • i ■ ■ ■ • i ■ • • ■ i ■ 7.40 7.60 7.80 8.00 15 m/z 96.95 9.02% 35 ,49 85 97 117 125 • • i • “ Tr > > i | ■ i'i > | 1 ri । । । ■ i1. . i . . .'.’i ....).. .'. ।. .।. m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #64841: 2-Propanone. 1.1-dichloro- 43 ■ ■ i • ■ ‘ ' i ■ ■ ■ ■ i • • • i ■ • • • i • 7.40 7.60 7.80 8.00 5000 m/z 81.8.5 8.17%

27 36 I 49 63 83 91 126 ' ‘ I ‘ ■ I 111 I I■I■ ■ I 1 1 11 I 1 miz-> 10 20 30 40 50 60 ' ‘ 70 80 ** 90 100 110 120 130 Abundance #4732: N-Acetylpyrrolidone ' A 1T 43 1 ‘ i ■ 7.40 7.60 7.80 8.00 m/z 82.90 7.32% 5000 99 127

m/z—> 30 .............. I l j f 1 i > | r > 1 1 | 1 10 20 30 40 .50 1. .. 70 II.90.J. ..... AAAAu 56 60 86 7.40 7.60 7.80 80 100 110 120 130 8.00 TIr

30643.D GCMS1126.M Fri Feb 01 10:47:45 2002 Page 2

NYC-WTC_0000 18452

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NYC-WTC_000018452Source: NYC Law Department, mirrored locally

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