GC/MS calibration data for sample 30643, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\DEC2701\30643.D Vial: 59 Acq On : 30 Dec 2001 5:02 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L • ********************************************************************* Peak Number 1 Silane, tetramethyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 7.61 2.80 ug/1 1384940 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 4 Pentane, 3/methoxy- 102 C6H140 036839-67-5 9 Abundance Scan 280 (7.614 min): 30643.D (-) m/z 73.0p 100.00% 73

5000 43 | I 1 1 1 | 1 Tl 1 I I I | T-r-j-r-r

103 87 7.20 7.40 7.60 7.80 8.00 37, |, 1 50 55 .61 67, । +r ■ • i ■ ■ ■ • i ■ ■ ■ ■ i • — .9nn/mBnnnkn ■ i • ■ ■ ■ i • • ■ ■ i ■ ■ • ■ i • ■ ■ ■ i ■ ■ m/z 43.00 31.75% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane, tetramethyl- 73

5000 i ■ • ■ 1 i r 1 1 1 1 1 1 1 1 1 1 7.20 7.40 7.60 7.80 8.00 45 m/z 45.0,5 11.36% 15 , .1 53. 59 I 88 ' ' i • ‘ • I ■ • • • i • ■ ■ ' | । l > ■ | 7 .4'1 7 ■ ■ ■ ■ । • 1 • ■ i ■ ' ' ■ I 1 1 ■ ■ I 1 1 1 1 I 1 1 "I ' l 1 ' miz-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #292: N-Ethyiformarnide 30 73 • » I « 1 । » * * * I * * * ' i * * * * i 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.05 10.97% 44 58 i — m/z-> 10 20 30 40 10 50 60 70 ■ ■ i ' 1 • ' I ' ■ ■ ■ i • ■ ' ■ i ■ ■ • ■ i ' ■ 80 90 100 110 120 Abundance #49423:1,3-Dioxolane, 2-(3-bromo-5,5,5-trichloro-2,2-dlmet =r*mummTPTTTTer 73 7.20 7.40 7.60 7.80 8.00 m/z 71.0p 6.96% 5000 45 55 67. ■ ■ ■ i ■ ' ■ 1 i 11 1 1 i 1 36.11'1......... 1'1m 4-t _______________ 109115 1144*1*11 TT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.20 f 7.40 17.60 7.80 8.00 '

30643.D GCMS1126.M Fri Feb 01 10:47:40 2002 Page 1

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