GCMS analysis results for sample AD30356, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2701\30356.D Vial: 21 Acq On : 28 Dec 2001 7:34 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Silane, tetramethyl - Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 7.62 4.04 ug/1 1355480 1,4-Dichlorobenzene-d4 11.68 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1,3-Dioxolane, 2-pentadecyl- 284 C18H3602 004360-57-0 9 4 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 280 (7.618 min): 30356.D (-) m/z 72.95 100.00% 73

5000 43 i ■ ■ • ' i ■ ■ • ■ i • Ip— i । । > । 7.20 7.40 7.60 7.80 8.00

m/z-> — L4 • ■ • । ■ 87 103 ■ i ■■ ■ i '* ■ ■ ■ i ■ ■ ■ • i'1 • • i • ■ ■ ■ i ■ ■1 ■ i ‘ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 • ■ i ■ ■ ■ ■ i ■ • • ■ i ■ ■ ■ ■ i ■ • m/z 43.00 30.76% Abundance #62932: Silane, tetramethyl- 73

5000 .. M.... 7.20 7.40 7.60 7.80 8.00 45 m/z 41.00 11.33%

. W. 15_____ J 59 88 ■ ■ i ■ ■ ■ ■ i miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #292: N- E thyiforman lido 30 73 1 7.20 7.40 7.60 7.80 8.00 5000 m/z 45.05 11.06% 44 58

15 , • ■ i • ■ ■ ■ i ■' i'''' i ‘ ' i1' ‘ ■ i ' ■ ■' i'' ‘' i' ■ ' ■ i ■ ‘ ‘ i ‘ ‘ ‘ i • ■ ■ ‘ i' ‘' ■ i' ■ ■ ■ i' ' m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #40191:1,3-Dtoxolane, 2-pentadecyl- [14** i rn"’ ■ । TTprrr| i r 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.84% 5000

43 57 86 99 _________________________________________________ 256 283 . ’ 1+*’’I’**’I’ • ‘ • 1***’IASI*’**I*S**I****IS*4411**I****IS+SIS-+1* [-r. i . । ■ t । . i i । n i“i“| । । m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 7.20 7.40 7.60 7.80 8.00

30356.D GCMS1126.M Wed Jan 02 10:57:06 2002 Page 1

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