GCMS analysis results for sample AE08014, April 2002

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Laboratory report documenting GCMS analysis of sample AE08014 conducted on April 24, 2002, including surrogate recovery data.

NYC-WTC_000047682–000047690

Folder label: “GCMS X 4/4/02 A 4/12/02”

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Data File : C:\HPCHEM\l\DATA\APR1102\8014.D Vial: 20 Acq On : 12 Apr 2002 9:03 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.83 0.42 ug/1 64706 Naphthalene-d8 15.87

Hit# Of 5 'entative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 37 3 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 Abundance Scan 1066 (14.829 min): 8014.D (-) m/ z 73.00 100.00% 73

5000 267 355 .................. | Ii i ।| I /..................... i r | I I I I | । I I| II I I

45 14.40 14.60 14.80 15.00 15.20 - 118 154 193 223 . TTTuam 323 . [ m/ z 267.00 47.86% ' ‘ I ' 1 " Arun)) I I ।‘| I । I r| i i i < । I i । i | I 1 I I | i > i > | i i . n/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 ...................... ,.......................... 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.05 39.64% 207 323 , r "' i" " i" " I" " I"ri I 1‘*AIII‘I***/***/d/m/ 1 r ■1 ■ T" "i n/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 ____________ 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 14.91% 44 ... Iiiliii""i 193 147267 294 TWTIPITITWITTTTT i""r"Ti r'" i m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #57357: Noradrenaline, tetra-TMS 73 T 14.40 14.60 14.80 15.00 15.20 m/ z 357.05 9.89%

5000 102 355

45 — 147 442 I i" " i" " i I* I | | |1' ’'| " j ' '"I । ■ 1 । | । । । > |T‘ ‘ I i ■ ' ‘ r i ' ' ■ ■ i ■ ■ ■ ■ i ■ ■ m/z—> 40 60 80 100120140160180200220240260280300320340360380400420440 14.40 14.60 14.80 15.00 15.20

8014.D GCMS0412.M Tue Apr 16 12:07:24 2002 Page 1

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GCMS analysis results for sample AE08013, April 2002 · Box DEP Box 27

NYC-WTC_000047673

Laboratory report documenting GCMS analysis of sample AE08013 conducted on April 24, 2002, including surrogate recovery data.

1 shared topics · Same agency, volume and box · similarity 0.999