GCMS analysis results, Sample AE08270, April 22, 2002

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GCMS analysis report for sample AE08270 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048456–000048465

Folder label: “GCMS X 4/9/02 A 4/17/02”

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Data File C:\HPCHEM\1\DATA\APR1802\8270.D Vial: 4 Acq On 18 Apr 2002 2:54 pm Operator: Sample Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.81 1.86 ug/1 265270 Naphthalene-d8 15.85

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 Phenethylamine,/N-methyl-.beta., 3,4 399 C18H37NO3Si3 010538-85-9 3 N-(Trifluoroac tyl)-0,0',0'1-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 4 Noradrenaline/ tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 Abundance Scan 1064 (14.810 min): 8270.D (-) m/z 72.95 100.00% 73

5000 267 355

I 1 I 1 1 I ’ ■ Td 1 45 14.40 14.60 14.80 15.00 15.20 103 133154 193.223 1 1 1 m/z->_____ 50 1 i 1 ■ r ■ 1’** 1 r'1 ''1 100 150 200 250 +1 293300 323 1 i 1 1 ' ■ i ■ 1 ' 1 i ■ m/z 355.05 48.28% 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 .................. / ..................... I ' ' ' ' I ' 1 1 1 I 1 ' 1 ' I ' 1 ' 1 I ' ' 14.40 14.60 14.80 15.00 15.20 m/z 267.00 45.61% .......... 207 । 323 , m/z-> 50 100 150 200 250 300 350 400 450 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 ..00000080100001111 14.40 14.60 14.80 15.00 15.20 5000 355 m/ z 3 56.05 16.79% 44 IL . 147 193 267 294 , ' ' i 1 ' 1 i ■ ■ 1 1 'i 1 ' ' ■ 1 1 ' ■ r i ‘ '■ ■ ‘‘ I 1 1 1 1 I 1 1 1 I"1 1 1 1 I ' nlz->_____ 50 100 150 2 00 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no /I I 1 ' ' ' I ' ' 73 14.40 14.60 14.80 15.00 15.20 m/z 267.90 12.86% 355 5000-

45 | | 126147 193 265 376 481 I \ TL 1 ’ i ■ 1 1 r i 1 ' ■ 1 i ' 1 1 ' i 1 । - r r . ■ ■ ■ । ■ 1■ । > । > । । । । > ' m/z—> 50 100 150 200 250 300 350 400 450 14.40 14.60 14.80 15.00 15.20

8270.D GCMS0412.M Fri Apr 19 08:30:57 2002 Page 2

NYC-WTC_000048464

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