GCMS sample analysis report, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN1 802\31550.D Vial: 16 Acq On : 19 Jan 2002 6:13 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Eicosane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

24.52 0.25 ug/1 71000 Phenanthrene-dl0 24.77

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 3 4 Eicos e Hepta .ecane Pen decane Oct .decane Abundance Va Scan 2122 (24.522 mln): 31550.D (-) 282 C20H42 240 C17H36 212 C15H32 254 C18H38 m/z 57.00 000112-95-8 000629-78-7 000629-62-9 000593-45-3 100.00% 91 91 91 90 57

miz-> 5000

Abundance 40 43

11T 111 60 71 85

1.... #..2113 127 141 155 80 100 120 140 160 180 200 220 240 260 280 #72323: Eicosane •04 A 24.20 24.40 24.60 24.80 m/z 43.05 73.67% ‘I

43 57

71 5000 85 24.20 24.40 24.60 24.80 ' m/z 71.10 61.78% f 99 113 127 141 282 1 ■ i ■ ■ ■ ■ i ■ ■ ■ • i ■ • ■ ■ i • ■ • ' i ■ ' ■ ■ i' 1 ‘ ' i 1 1 ‘ i ' ' ' ' i ' ' ' ■ i ' ■ ' ■ i ■ T-j-n-n-p-r m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 71191: rigotadachm . 57 43 71 LA24.20 24.40 24.60 24.80 5000 m/z 85.05 38.65% 85

.. .......................................... . ........ . miz-> Abundance 40 60 80 100 120 140' 160 #26001: Pentadecane 180 200 220 240 260 280 . /A./ t > , 43 57 24.20 24.40 24.60 24.80 71 m/z 41.05 36.42% 5000 85

99 -n-p-r d.a113127 I ‘ ‘ 1 4 ! ‘ ........ 168.......... 212........................ ’ * I ‘ ‘ r‘ I ' ‘ ‘ ' I ‘ ‘ ‘ 4 I ‘ ‘ ' I * ‘ ‘ ‘ I ' ‘ 1 ‘ I ’ ' ‘ • t ‘ ’ ‘ * I • ' * ‘ I ‘ ‘ RA-) N V WwA • ‘i • ■ ■ ■ 1 1 11 ' i 1 1 '1 i 1 1 1 1 i m/z-> 40 60 60 100 120 140 160 160 200 220 240 260 280 24.20 24.40 24.60 24.80

31550.D GCMS0103.M Wed Feb 06 15:41:01 2002 Page 2 NYC-WTC_000016675