GCMS comments for sample AD29785 detecting phthalate, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29785.D Vial: 5 Acq On : 15 Dec 2001 6:26 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ***************************************************************** * ** * Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

11.34 0.74 ug/1 179356 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative" ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2 1-Propanol, 2-(2^hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 3 2-Butanol, 3,3/-oxybis- 162 C8H18O3 054305-61-2 42 4 2-Propanol, 1,1‘-oxybis-_________ 134 C6H14O3 000110-98-5 39 Abundance Scan 686 (11.345 min): 29785.D (-) m/z 59.05 100,. 00% 59

5000

m/z-> 20 —Al— 30 40 45

50 - 60 70 73

80 84 90 103

100 110 120 130 140 ■ • i ■ ' 11.00 11.20 11.40 11.60 m/z _N 44.95 52.26% ■ ■ i •

Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 103 45 11.00 11.20 11.40 11.60 73 31 m/ z 103.00 33.37% ■ । । ■ ।' ■ • • । ■ ■ • • । • |....... ... i...... 130 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Propanol, 2-(2-hydroxypropoxy)- 59 • • । ■ k i ■ • ’ i ■ ■ ■ • i 1 ' ■ ■ i ' 11.00 11.20 11.40 11.60 5000 m/z 73.00 30.74% 31 45 103

| ii 75 89 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3‘-oxybis- T T— 59 11.00i 11.20 11.40 11.60 m/ z 41.05 28.74% 5000 31 45 103

----- , I , .......... 134 , tmmmT TOT I I I I1 m/z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60

29785.D GCMS1126.M Fri Dec 28 13:20:03 2001 Page 3

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