GCMS comments for sample AD29785 detecting phthalate, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\DEC14 01\29785.D Vial: 5 Acq On : 15 Dec 2001 6:26 am Operator: 209 GALOS Sample : gems scan 12/10 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.43 0.79 ug/1 193285 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tent at ive/ID MW MolForm CAS# Qual

1 2-Propanol, 1- (2-methoxy-1-methylet 148 C7H16O3 020324-32-7 83 2 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 50 3 2-Pentanone, 5 methoxy- 116 C6H1202 017429-04-8 45 4 1-Propanol, 2/(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 42 Abundance Scan 695 (11.427 min): 29785.D (-) m/z 59.05 100.00% 59

miz-> 5000

20 ...... .................. 30 _ 40 45

50 60 70 73

80 89 TTu 90 103

100 110 120 130 140 11.00 m/ z 11.20 45.0.0 N 11.40 11.60 11.80 48.63% Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy}- 59 J 5000- 45 103 11.00 11.20 11.40 11.60 11.80 73 31 m/ z 103.05 37.69% -- mp . i1 j . . IIT ........... ,.......... 130 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #12859: 2-Butanol. 3,3°-oxybis- 59 11.00 11.20 11.40 11.60 11.80 5000- 31 m/ Z 73.00 30.14% 45 103 I

i • i ■ ■ r i ■ I J ..... ................ 134 , 1 1 1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #64282: 2-Pentanone, 5-methoxy- TBnf—mm TInnmmmmgg 43 59 11.00 11.20 11.40 11.60 11.80 m/ z 41.05 28.21%

5000

69 — — L... 84.... 101 116...... J n-1 m/z--> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.00 11.20 11.40 11.60 11.80

29785.D GCMS1126.M Fri Dec 28 13:20:08 2001 Page 4

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