GCMS analysis results for sample AD25946, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2101\25946.D Vial: 12 Acq On : 21 Nov 2001 10:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Propane, 2-ethoxy- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.08 1.49 ug/1 360468 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propane, 2- ethoxy- 88 C5H120 000625-54-7 40 2 1,2-Propanediol, 3 -methoxy- 106 C4H10O3 000623-39-2 36 3 2,3-Butanediol 90 C4H10O2 000513-85-9 33 4 2-Butanol/ 3-methyl- 88 C5H120 000598-75-4 9 Abundance Scan 222 (7.079 min): 25946.D (-) m/z 45.05 100.00% 45

5000 61 73 1 ri ■ 11 TITur 1 ‘ 1 * 1 1 1 1 1 1 ____ 6.80 7.00 7.20 7.40 miz-> TT 36 । 4... Arer... 111, ■ h {,,, > । 207 । । । । ■ ■ ■ > । < <, > । . 1111111111111 n 1111 n'> 1111' 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 m/z 43 " 71.49% Abundance #62956: Propane, 2-ethoxy- 45

5000 ’ ‘ 1 ‘ 1 * ‘ ‘ ‘ I ‘ ‘ ‘ * I ' ‘ ‘ i * ‘ ‘ 1 73 6.80 7.00 7.20 7.40 15 27 m/z 61.05 35.26%

miz—> LX tttm 59 1 TYpT 88 TTggmp 10 2030405060 70 8090 100110120130140150160170180190200210 I’T Abundance #836 1,2-Propareaiol I.metnony- 45 rrr T 113 TTT . ITT11100/0/0 6.80 7.00 7.20 7.40 m/ z 73.00 32.09%

.1 5000 75 31 61 15 I 88

miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130140150160170180190 200210 Abundance #917: 2,3-Butanediol.. ....... . rrrr1’ TI i 1 11r i 45 6.80 7.00 7.20 7.40 m/ z 44.00 17.47%

1 m/z-> 5000

-59 57 29 .. .... ..... 19

10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 L ■ ■ i ■ • • ■ i ■ ■ • • । 111 111 1 6.80 7.00 7.20 7.40

25946.D NP103001.M Tue Dec 11 09:30:23 2001 Page 1

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