GCMS analysis results for sample AD25947, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV2101\25947.D Vial: 8 Acq On : 21 Nov 2001 6:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Propane, 2-ethoxy- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.06 1.05 ug/1 243847 1,4-Dichlorobenzene-d4 11.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Propane, 2-ethoxy- 88 C5H120 000625-54-7 40 2 2,3-Butanediol 90 C4H10O2 000513-85-9 28 3 2-Butanol,/3-methyl- 88 C5H120 000598-75-4 9 4 Guanidine, methyl - 73 C2H7N3 000471-29-4 7 Abundance Scan 220 (7.060 min): 25947.D (-) m/z 45.00 100.00% 45

5000 61 73 TTTrrTTT • i • • ■ • i ■ • ■ 36 41|, 51 88 6.80 7.00 7.20 7.40 78 1111 pi 111 r> 1111 n r]"i< > r | n T | > n TITTu TIWa m/z 43.0, 75.61% miz-> 5 10 15 20 25 . 30 35 40... 45 50 55 60 65 70 75 80 85 90 95 Abundance #62956: Propane, 2-ethoxy- 45

— 5000 ‘ 1 Li 1 ‘I Li ‘ TITTT TII ’ ’ 73 6.80 7.00 7.20 7.40 15 27 m/z 73.00 32.08% 39 59 88 - Hpp TOga miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 •Abundance #917 2,3-Butanediol 45 CTTngt1 ITTrt I T' T ‘ 6.80 7.00 7.20 7.40 5000 m/z 61.00 31.60%- 29 - —19 1 i 75 90 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62961: 2-Butanol, 3-methyl- — r. II TP , — 4(5 6.80 7.00 7.20 7.40 m/z 44.00 1 6.50% 5000

27 I 55 73 ppm tmmmmmm ‘ I • i • • • | i • • • | • i i i • • m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 . 6 80 7.00 7.20 7.40

25947.D NP103001.M Tue Dec 11 09:31:23 2001 Page 1

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