GCMS method parameters and calibration table, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\LB.D Vial: 2 Acq On 18 Dec 2001 4:49 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Hexanone Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.60 0.57 ng/uL 156770 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 90 4 2-Hexanone 100 C6H120 000591-78-6 90 Abundance 7 . Scan 191 (6.597 min): LB.D (-) m/z 43.10 100.00% 48

58 5000 -

71 85 100 MA 6.20 " i r 6.4G । ■ ' ■ TT 11 • T ■ 6.60 6.80 7.00 P+ TDT TtmpT T1 1 — r'" i m/ z 58.10 53.96% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #63384:2-Hexanone 43

5000 58 'I...... AA 6.20 6.4G 6.60 6.80 7.00 29 m/ z 41.10 18.31% 39 miz-> m 1111111111' I 71 85 100 P— 1111111 • 111" 11"1 |i m 11" 11 hi i|1 11 I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63385: 2-Hexanone 43 —A—4 -------- 6.20 6.40 6.60 6.80 7.00 5000 - 58 m/z 57.10 15.45% 29 1 I 39 | 71 85 100 TTTTTT TIT PPWON TT • r •" i"'11 • •" i"1 • i • •1 ’ 11 • TTTTTTTT i • ■ ■ ■ i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance 43 #1556: 2-Hexanone D 4 A A...... 6.20 6.40 6.60 6.80 7.00 m/z 39.10 8.39% 58 5000- A 27 39 71 85 100 - — mH ■ • i ■ ■ ■ • 11 • I • • > • i ■ ■ • ■ | • • ■ ■ ।‘ |1 11 ■ ‘ ‘41 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

LB.D NP112701.M Thu Dec 20 11:37:55 2001 Page 1

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