GCMS calibration data, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28171.D Vial: 37 Acq On : 22 Dec 2001 1:59 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Cyclohexane, azido- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.76 0.58 ng/uL 152474 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, azido- 125 C6H11N3 019573-22-9 28 2 2-Butenal, 3-methyl- 84 C5H80 .. 000107-86-8 25 3 2,4,6,8-Te ramethyl-1-undecene 210 C15H30 059920-26-2 9 4 2-Propanone, 1-(1-methylethoxy)- 116 C6H12O2 042781-12-4 9 Abundance 7 Scan 645 (10.759 min): 28171.D (-) m/z 43.10 100.00% i • 43 83 / 55

5000

— 71 -AA 10.40 10.60 10.80 11.00 1 . m/z-> 20 ................ 30 —4 40 tn 50 60 70 80 90 100 110 120 130 m/z 83.15 79.72% Abundance #4321: Cyclohexane, azido- 83 55 41 5000 TT ) + 10.40 10.60 10.80 11.00 Tr 27 m/z 66.11%

m/z-> 20 ■ i • ■ ’ ■ i...... i 30 40 ' I 1 50 - 4.. 60 67

70 80 , 96 Tr ' i 1 ' 1 ■ i ■ ' ' 1 1 1 90 100 110 120 125 130 55'10 Abundance #559: 2-Butenal, 3-methyl- . 55

83 ■ I • A + 10.40 10.60 10.80 11.00 I" 39 5000 m/z 41.10 25.46% 27

| 69 ।• ■ i ' ■ ■ ■ i ■ ■ ■ ‘ i ' ' ■ ' i ■ ' ■ ■ i ' ' ■ ■ i ■ ' ' ' i 1 1 ■ • । • i • ■ ■ ■ i ■ । ■ • , ■ • • ■ i ■ ■

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 - Abundance #25485: 2,4,6,8-Tetramethyl-1-undecene 1 43 10.40 10.60 10.80 11.00 m/z 71.05 22.61% 29 5000 55 69

miz-> ■ i ■ ■ ' ■ i ■ ' ■ ' i 20 30 40 I —. I---—...—... - 50 ! 60 70 11 80 83 90 100 110 120 130 ‘I 10.40 10.60 10.80 11.00

28171.D NP112701.M Fri Dec 28 09:07:45 2001 Page 6

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