GCMS analysis results for sample AD27679, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27679.D Vial: 6 Acq On : 19 Dec 2001 11:43 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Cyclohexane, bromo- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

10.82 1.18 ng/uL 262105 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Cyclohexane , bromo- 162 C6HllBr 000108-85-0 33 2 2-Butenal, 3-methyl- 84 C5H80 000107-86-8 9 3 Butane 58 C4H10 000106-97-8 9 43-Methyl-1-[(1H)-1,2,4-triazol-1-yl 153 C7H11N30 064922-02-7 9 Abundance Scan 652 (10.818 min): 27679.D (-) m/ z 43.10 100.00% 43 83 55

5000-

71 ntinl A m/z-> 10 —.................... 20 30 40 l d TIE 4—— 50 60 70 80 90 100 110 120 130 140 150 160 170 m/z i' * *' i'''' i'' ■ * I' • ■11 r 10.40 10.60 10.80 11.00 11.20 83.15 84.18% Abundance #67630: Cyclohexane, bromo- 83

5000- 55 10.40 10.60 10.80 11.00 11.20 m/ z 55.10 69.05% .......... 27............. 4 67 162 —........... 4 i • ■ • • i • ■ • • । Ti TTTTTr m/z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #559: 2-Butenal. 3-methyl- 55 ! — -------- ! 83 10.40 10,60 10.80 11.00 11.20 39 5000 m/z 41.10 26.99% 27

I j t. . 69। h . r . ।। TIETTTTTTTTT I •'1' I TT m/z-> 10 20 30 40 50 60 70 80 90 100 11C 120 130 140 150 160 170 Abundance 6: utane -- 43 10.40 10.60 10.80 11.00 11.20 m/z 71.05 17.38% 5000 29

m/z--> 15 - '111 10 20 30 ++ 40 50 58

60 70 80 90 100 110 120 130 140 150 160 170 AA —A TEEEETE1-IT 10.40 10.60 10.80 11.00 11.20

27679.D NP112701.M Thu Dec 20 11:42:26 2001 Page 13

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