GCMS analysis results for sample AD28168, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2101\28164.D Vial: 14 Acq On : 22 Dec 2001 5:46 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Cyclohexane, bromo- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.76 0.93 ng/uL 270070 1,4-Dichlorobenzene-d4 11.79

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

I Cyclohexane, bromo- 162 C6HllBr 000108-85-0 33 2 2 - Nonanone,9 - hydroxy - 158 C9H18O2 025368-56-3 10 3 1 - Pentene, 4 -methyl - 84 C6H12 000691-37-2 9 4Butane 58 C4H10 000106-97-8 9 Abundance Scan 645 (10,760 min): 28164.D (-) m/ 100.00% 43 83 55

5000 TI—nDDBn/ 71 10.40 10.60 10.80 11.00 - ■•i"■■r "■r miz-2 ____ 10 20 30 T T l' " ' I' +IPTTITTITTTTTTTTTTTTTTTTTTTTT 40 50 60 70 80 90 100 110 120 130 140 150 160 170 m/z 83.15 84.97% Abundance #67631: Cyclohexane, bromo- 83 —.................... 5000 55 TITr ' T 10.40 10.60 10.80 11.00 m/z 55.10 69.89% 27 67 J 164 l. j .... 11».. 1111.11 ।, । T 1111 i'i 1111 TIT 4 "I" T‘IUTTIIITTTT*"*IIITI‘ miz- 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #11995: 2-Nonanone, 9-hydroxy 43 58 ............ I ' 10.40 10.60 10.80 11.00 5000 m/z 41.10 25.08% 71 82 TIWWTuupununu i1 •'11 i•"1r•"i i " ■ ■ r ■ ■ ■ i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #599:1-Pentene, 4-methyl- 1 Pmgr TIT 43 10.40 10.60 10.80 11.001 '

m/z 39.10 14.63% 5000 56 27 69 84 15 । | । । । | । | ’ • > ' |" Tupu 1__ -.............. 4 miz-? 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 10.40 10.60 10.80 11.00

28164.D NP112701.M Fri Dec 28 09:56:33 2001 Page 8

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