GCMS analysis results for sample AD28166, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC21O1\28165.D Vial: 15 Acq On : 22 Dec 2001 6:40 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 Cyclohexane, bromo- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.76 1.06 ng/uL 284314 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, romo- 162 C6HllBr 000108-85-0 38 2 3 -Methyl -1- (1H)-1,2,4-triazol-1-yl 153 C7H11N30 064922-02-7 36 3 N,N' -Bis. (2, 6-dimethyl-6-nitrosohept 338 C18H30N2O4 066737-12-0 28 4 Cyclohe .ne. bromo- 162 C6HllBr 000108-85-0 28 Abundance Scan 645 (10.759 mln): 28165.D 0 m/ 43.10 100.00% 43 83 55

5000

71 10.40 10.60 10.80 11.00 - ..... ... + • । । । । ....... . 11 u' 1111111 m/z 83.15 93.00% miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #67630: Cyclohexane, bromo- 83

5000 55 ----- 10.40 10.60 10.80 11.00 m/z 55.10 70.40% 27 : 67 ।162 TT—U——nng " 11 r 11" " I'1111'1 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #10506: 3-Methyl-1-[(1H)-1.2.4-triazol-1-yilbutan-2-one 43 83 -A -......... 10.40 10.60 10.80 11.00 5000 71 i m/ 41.10 29.62% 55 I 154 TI... —I T-p-n-rprT-rp-n , , "‘‘11111017111011u—ITT‘‘ICTIITTIr n/z-> Abundance 20_ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 #47904: N,N-Bis(2,6-dimethyl-6-nitrosohept-2-en-4-one) 83 4 1 n 1 11 i1 1 ■111 10.40 10.60 10.80 11.00 m/z 71.05 14.80% 5000 55

29 39 1 I ' ' ’ ' 1 ‘ - ■ 11+. ।।11 Ti _1111′11′11991TTTTtuuukTTDTu 123 139 —0—09‘ivuuTUu A A • I ' ' ' 'I ' ' ’ ■ ■ i ■ ■ ■ ■ । ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 10.40 10.60 10.80 11.00

28165.D NP112701.M Fri Dec 28 09:57:19 2001 Page 8

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