GCMS analysis report, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report.

Data File C:\HPCHEM\1\DATA\DEC2101\28309.D Vial: 41 Acq On 22 Dec 2001 5:37 pm Operator: GALOS Sample gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Cyclohexane, bromo- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

10.75 0.71 ng/uL 183886 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, omo- 162 C6HllBr 000108-85-0 40 2 Cyclohexane/ bromo- 162 C6HllBr 000108-85-0 33 3 Cyclohexane, azido- 125 C6H11N3 019573-22-9 33 4 1-Methyl 1H-1,2,4-triazole 83 C3H5N3 006086-21-1 9 Abundance Scan 645 (10.753 min): 28309.D (-) 43.10 100.00% 43 83

A 55 5000

71 10.40 10.60 10.80 11.00 i 'm/z-> —l —ll 20 30 40 50 60 I70 — IIT m/z । rr. i| । ( . । । । । । i| । ri । । । i । । । । । । >|

80 90 100 110 120 130 140 150 160 170 83.15 73.89% Abundance #12779: Cyclohexane, bromo- i 83 55 \.......... 5000- 10.40 10.60 10.80 11.00 27 m/ z 55.10 66.53% 67 | I ‘T‘ ■' r TT 1,11 — 11' ' •»’ 1111′111111′1111 164 i '' ■' i ■ m/z-> 20 30 40 50 60 . 70 80 90 100 110 120 130 140 150 160 170 Abundance #67630: Cyclohexane, bromo- 83 A 1" i • ■ ■ 10 40 10.60 10.80 11.00 5000 55 m/z 41.10 24.16%

27 67 12‘"‘1110‘-1CTEIT"I1101IIIIr T"IE‘I‘EEITEEEITEETII 162 1 i 1 1'' r 1'111 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #4321: Cyclohexane, azido- L ----- f I 83 10.40 10.60 10.80 11.00 55 m/ z 71.05 16.57% 41 5000- 27 67 - 96 125 —A—M m/z-> 20 30 40 58 60 70 — TIT ' ' 1 ' i ‘ 1 ' ' I 1 1 1 1 I 1 1 ‘ ’ I 80 90 100 110 120 130 140 150 160 170 TT 10.40 10.60 10.80 11.00

28309.D NP112701.M Fri Dec 28 09:10:18 2001 Page 6

NYC-WTC_000035409