GCMS analysis report, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2101\28309.D Vial: 41 Acq On : 22 Dec 2001 5:37 pm Operator: GALOS Sample : gems unknown 11/26 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 2-Pentanol, 4-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

10.43 0.82 ng/u: 212889 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol/ 4-methyl- 102 C6H140 000108-11-2 43 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 38 3 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 38 4 2-Hexanol 102 C6H140 _______ 000626-93-7 35 Abundance Scan 610 (10.432 min): 28309.D (-) m/z 43.10 100.00% 43

m/z-> 5000

10 I ■11 ■ 1" 111 ■ " • 1'1 15 20 25 ' i ■ 30 35 39 —4 146... +l ...........-........ 40 45 50 55 60 65 70 57 61 69

75 85 — 80 85 90 95 - -----A 10.00 m/z 10.20 10.40 10.60 10.80 45.10 1 67.52% Abundance #1773: 2-Pentanol, 4-methyl- 45

5000 TTT ' ' Ar TIIr 10.00 10.20 10.40 10.60 10.80 69 m/z 41.10 29.10% 27 4; 57 | 84 87 f “ ----- mTPHm 11 •'1 ■ i' ■11111" 1111111111111 m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546; 2-Pertanol. 4-methy- 45 A — r10.40 — 10.20 10.00 Ar 10.60 10.80 5000- m/ z 85.15 19.72% 27 19 , 31 57 42,1 69 84 87 1 “ ■ i ■ • ■ ■ i ■ ■ i ■1"।।i•'TTTTTT 11111111 ‘ TTTTT 11111111 ■ ।■ ■ ■ ■ । " i1'" i"111" m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 'Abundance #63547: 2-Pentanol, 4-methyl- A - T "I 45 10.00 10.20 10.40 10.60 10.80 m/z 57.10 15.96% 5000

27 69 .............. 1 38 41 I [ I > >«11 ‘TTTTT > I I I til I I I I I I « I { I I t I I I I I ‘IT 57 THT ' " I " ' '| I TTTT I 1 1 । 1 1 1 1 84 87 11 I ' 1 1 1 1 । 1 ' 1 1 1 1 T.I." i A IF m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 10.00 10.20 10.40 10.60 10.80

28309.D NP112701.M Fri Dec 28 09:10:16 2001 Page 5

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