GCMS analysis results for sample AD27678, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27678 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033247–000033262

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01”

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NYC 9/11 Public Portal Document

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.Data File : C:\HPCHEM\1\DATA\DEC19O1\27678 .D Vial: 5 Acq On : 19 Dec 2001 10:48 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Methyl-1-[(1H)-1,2,4-triazol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.81 1.10 ng/uL 265436 1,4-Dichlorobenzene-d4 11.85

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Methyl-1-[ (XH) -1,2,4 - triazol-l-yl .153 C7H11N30 064922-02-7 23 2 Cyclohexane/azido 125 C6H11N3 019573-22-9 17 3 Cyclohexane, bromo- 162 C6HllBr 000108-85-0 12 4 Cyclohexane, bromo- 162 C6HllBr 000108-85-0 12 'Abundance Scan 651 (10.809 min): 27678.D (-) m/z 43.05 100.00% 43 83 55 5000- 71 X TTITTTTPT 1 11 11 1 1

m/z~> 20 m 30 40 TT ' 1'" —+ 50 60 70 • । r ■ ।' 80 90 11'1 ■ 111 ■' i ■' ■ ■ i ■ ■ ■ ■ i ■'' ■ i 100 110 120 130 140 150 160 170 10.40 m/z 10.60 10.80 11.00 11.20 83.15 71.40% Abundance #10506: 3-Methyl-1-[(1H)-1,2.4-triazol-1-yl]butan-2-one 48 83 / 5000 71 TTP i 10.40 10.60 10.80 11.00 11.20 55 m/ z 55.10 60.87% . 154 TI--PP P—IT i • ■ > ■ i • • ■ ■ i i ■ ■ • ■ i T‘ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #4321: Cyclohexane, azido- । 83

41 55 MU ■ ■ i • • ■ > i ■ ■ ■ ■ । 10.40 10.60 10.80 11.00 11.20 ■

5000 m/z 71.05 25.52% 27 67 .................... — ,1 — 96 125 III m/z-> 20 30 40 50 60 70 30 90 100 110 120 130 140 150 160 170 Abundance #67632: Cyclohexane, bromo- N । ■ ■ ■ ■ । TE A 83 10.40 10.60 10.80 11.00 11.20 m/z 41.10 23.70% 5000 55

m/z-> 20 30 40 50 m— 60 67 70 80 164 I T‘UUI1"CC—nrtptttiTm-rp-mT’turOnr 90 100 110 120 130 140 150 160 170 \ / I r 1 11 1 ' TTAItPr 10.40 10.60 10.80 11.00 11.20

27678.D NP112701.M Thu Dec 20 11:41:18 2001 Page 7

NYC-WTC_000033261

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GCMS analysis results for sample AD27627, Jan 2002 · Box DEP Box 21

NYC-WTC_000033143

Laboratory report documenting GCMS analysis of sample AD27627 for unknown compounds and surrogates on January 3, 2002.

1 shared topics · Same agency, volume and box · similarity 0.999