GCMS analysis results for sample AD28104, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28167.D Vial: 17 Acq On : 22 Dec 2001 9:25 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library 1 C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Methyl-l-[(1H)-1,2,4-triazol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.76 0.86 ng/uL 188659 1,4-Dichlorobenzene-d4 11.78

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Methyl-l- 1H)-1,2,4-triazol-l-yl 153 C7H11N30 064922-02-7 36 2 Cyclohexane; azido- 125 C6H11N3 019573-22-9 33 3 Cyclohexane, nitro- 129 C6H11NO2 001122-60-7 12 4 1,4-Pentadien-3-ol______ ____________ 84 C5H80 000922-65-6 9 Abundance Scan 645 (10.757 min): 28167.D (-) 43 710 100.00%| 43 55 83 m/3 5000

m 71 1 90 100 110 'l2o‘ 130 140 150 160 1T ' I''' '1 | । । n i । । । । —— _A 10.40 10.60 10.80 11.00 m/z 83.15 76.16 miz-> 20 30 40 50 60 70 80 Abundance #10506: 3-Methyl-1 -[(1 H)-1,2,4-triazol-1 -yl]butan-2-one 43 83

5000 71 ' ' i' i ' -------- 10.40 10.60 10.80 11.00 55 m/ z 55.10 72.86% TITT 154 । 19— . . .. "V" I 11 ‘ 11’111 I""I■ miz-2 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #4321; Cyclohexane, azido- 83 55 —— 41 10.40 10.60 10.80 11.00 5000 m/z 41.10 29.03% 27 67 ।.... ,, 96 . 125 i —IPP ' i'' " i' ■ • ■ i' i ■ ■'' i ■ miz- 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #5214: Cyclohexane, nitro- \ TMPT--TT 55 f T 10.40 10.60 10.80 11.00 83 m/z 71.05 15.60% 41 5000

27 67 TITTTLTTTT PT’r +.... 4.....1 t ■ i • < ■ ■ i ■ ■ ■■।■111111' i ■ ■ ■ ■ । ■■■■।■■■ ■ । ■ - —........................ miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 10 40 10.60 10.80 11.00

28167.D NP112701.M Fri Dec 28 09:58:16 2001 Page 7

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