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GCMS analysis results for sample AD27544, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD27544 for unknown compounds and surrogates on December 18, 2001.

NYC-WTC_000033417–000033432

Folder label: “GCMS X 11/15/01 A 12/13/01

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Scanned page image, NYC-WTC_000033431
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\27544 .,D Vial: 3 Acq On : 13 Dec 2001 12:12 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Methyl-1-[(1H)-1,2,4-triazol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

10.83 0.54 ng/uL/ 206815 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Methyl-1-[/1H)-1,2,4-triazol-1-yl 153 C7H11N30> 064922-02-7 23 2 2,3,3-Trime/hyl-1-hexene 126 C9H18 000000-00-0 17 3 Cyclohexane, bromo- 162 C6HllBr 000108-85-0 17 4 2,7-Octanedione______________ 142 C8H14O2 001626-09-1 12 Abundance < Scan 653 (10.828 min): 27544.D (-) m/z 43.10 100.00% 43 83 55 5000 71 i • ■ ■ ■ ।1 ’

m/z-> 20 — 30 40 —l 50 60 .I T 70 i' '' ' i' ■ ■ ■ I 90 100 110 120 130 140 150 160 170 80 I" 10.40 10.60 10.80 11.00 11.20 m/z 83.0,5 70.86% Abundance #10506: 3-Methyl-1-[(1H)-1,2,4-triazol-1-yl]butan-2-one 43 83

5000 71 10.40 10.60 10.80 11.00 11.20

55 m/z 55.1,0 59.22% .......... -- 154 ■ i ■ • ■ ■ i ' ■ ■ i’i ' ‘I" i' '' 11 !I i 1 1 ■ ■ i I '' '' I i" m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #4616: 2,3,3-Trimethyl-1 -hexene 55 83 I TIIIT — 69 10.40 10.60 10.80 11.00 11.20 5000- m/z 71.0,5 30.79%

27 1 - 97 111 ■ ■ i ■ '' ' 11 ‘ i ' ' '' i T" m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #12779: Cyclohexane, bromo- —।। > A , । A- - — 83 10.40 10.60 10.80 11.00 11.20 55 m/z 41.10 27.45% 5000

27 67 - T TT 164 ■ i'' '' i ■''' i'''' i' । i ' ■ ' ' i ■ ' ■ ' i i ■ । • ■ i i ' ■ '' f' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 10.40 10.60 10.80 11.00 11.20

27544.D NP112701.M Fri Dec 14 12:54:00 2001 Page 7

NYC-WTC_000033431

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NYC-WTC_000033431Source: NYC Law Department, mirrored locally

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