GCMS analysis results for sample AD28164, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\LB.D Vial: 10 Acq On : 22 Dec 2001 2:07 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 3-Methyl-l-[(1H)-1,2,4-triazol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

10.77 0.56 ng/uL 120862 1,4-Dichlorobenzene-d4 11.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Methyl-l-[(1X)-1,2,4-triazol-l-yl 153 C7H11N30 064922-02-7 33 2 2-Butenal, 3-methyl- 84 C5H80 000107-86-8 9 3 1,4-Pentadi n-3-ol 84 C5H80 000922-65-6 9 4 Butane / 58 C4H10 000106-97-8 100.00% 9 Abundance Scan 646 (10.769 min): LB.D (-) m/ 43.10 43 55 83 i ! 5000 - 71 J. V. / 7. V Tffrf ’ I ' ' ' ' I ' ' ' ' I '

m/Z-> 20 -+ ..... a— 30 40 50 60 ITT 70 80 90 100 110 120 130 140 150 160 10.40 10.60 10.80 11.00 11.20 m/z83.15 81.73% Abundance #10506: 3-Methy-1-[(1H)-1,2,4-triazol-1-yl]butan-2-one 43 83

5000 71 T TT| 10.40 10.60 10.80 11.00 11.20 |

55 m/z 55.10 71.86% 154 1 ■ ■ । ■ ■ ■ ■ । ■ m/z-> 20 30 40 50 60 ' 70 80 160 90 100 110 120 130 140 150 Abundance !lutonal, 3-mlf . 55 A 1 I ' ' TT 83 10.40 10.60 10.80 11.00 11.20 39 5000 m/z 41.10 29.24%) 27 । 69 • i ■ ' ' ' i ■ ■ ■ • i • ■ ■ ■ i ■ • ■ ■ i1 • ■' i • ■ ■ ■ i ■ 1 ■ • i ■1' ■ i ■ ' ■ ■ i ■ ■ ■ ■ i ■ • ■ ■ i ■ ■ ■' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ miz- Abundance 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 AA L #554: 1,4-Pentadien-3-ol 83 ■ i ■ ■ ■ ■ i • • 4........... — : 55 10.40 10.60 10.80 11.00 11.20 j m/ z 23.28% 71.05 5000 39 27 ! L 65 111'1 ' i' H..... -H TT 111 1 miz- 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 10.40 10.60 10.80 11.00 11.20

LB. D NP112701.M Fri Dec 28 11:46:59 2001 Page 9

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