GCMS analysis results for sample AD28164, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\LB.D Vial: 10 Acq On : 22 Dec 2001 2:07 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 2-Pentanol, 4-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

10.45 0.54 ng/uL 116114 1,4-Dichlorobenzene-d4 11.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 25 2 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 23 3 2-Hexan 1 102 C6H140 000626-93-7 23 4 Hexane, 1 -propoxy- 144 C9H20O 053685-78-2 17 Abundance Scan 611 (10.448 min): LB.D (-) m/z 43. 0 100.00% 43

5000

57 69 85 ‘ T 1 ' ' 'I' I' 1 39 61 10.20 10.40 10.60 10.80

miz-? 20 TTITTTTTTTTTTTTT 25 30 35 40 —3+4HT M 75 80 85 90 95 45 50 55 60 65 70 ' i1''1 r ■'' i'1'' i1''' r ' m/z 45.10 66.36% Abundance #1773: 2-Pentanol, 4-methyl- ! 45

5000 -4.. A— 10.20 10.40 10.60 10.80 69 m/z 41.10 28.91% ............... 27 44, ' ■ i ' ■ ■ ■ i ■ ■'' i ■' ■' i' ■' ■ i ■''11 57 ■ I •" ■ ■ I ' ■ ■ ■ l 1 ■ • ■ I • ; 84 87 • I' ’' ’ I'' '' I •'' 11 ‘' I'1 '' I'' m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 45 A -A- 10.20 10.40 10.60 10.80 4— 5000 m/z 85. ,5 19.51% 27 69 38 42, , 57 84 87 ■ i ■ ■' ■ i ■ ■ ■ ’ i ” " i' ■ ” i ■ ■ • ■ r miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 'Abundance #63583: 2-Hexanol T \ A 45 T T 10.20 10.40 10.60 10.80 m/z 57.10 16.04% 5000

- 69 1 .... 2731.....3942.1 • । 55 58 | " r11 ■ ■ i ■ ■ ■ ■ ........................... .. ..... 84 87 • 11' 11) 111111111111 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 10.20 10.40 10.60 10.80

LB.D NP112701.M Fri Dec 28 11:46:57 2001 Page 8

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