GCMS analysis results for sample AD28164, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\LB.D Vial: 10 Acq On : 22 Dec 2001 2:07 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 1-Butanol, 2,2-dimethyl- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

10.24 0.44 ng/uL 95992 1,4-Dichlorobenzene-d4 11.80

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanol. 2,2-dimethyl- 102 C6H140 001185-33-7 9 2 2,4,6,8-Tetramethyl-1 -undecene 210 C15H3 0 059920-26-2 9 3 DL-3,4YDimethyl-3,4-hexanediol 146 C8H18O21 032388-94-6 9 4 Butanal, 3,3-dimethyl-2-oxo-, hemih 114 C6H10O2! 077572-68-0 9 .Abundance- Scan 588 (10.237 min): LB.D (-) - I1 m/ z 43.10 100.00% 43 !

5000

39 55 59 73 85 .............. .............. A 9.80 W 10.00 10.20 10.40 10.60!

m/z-> - + 20 25 30 35 40 1..... — -H 45 50 55 60 65 70 75 80 85 90 95 m/z ’ 55.10 34.38% Abundance #63536 1-Butanol, 2,2-dimethyl- 43 71

5000 55 9.80 LA 10.00 10.20 10.40 10.60 m/ z 59.10 33.17%! 27 31 ||| 87 > > । ■ 11—————— i—unn—nu—nuannunum Ti j m-r TWTTTTTTT TII T m/z-> 20 25 30 35 40 45 50 55 60__ 65 70 75 80 85 90 95 Abundance ndocon 43 TIT 29 9.80 10.00 10.20 10.40 10.60 5000 m/ z 41.10 33.01% 55 69 39 ' 83 11 • ’1 • ।1 1IU0u——uutuuunu—9on‘]uunupuuuuwuuu]nuw*guuu9yuwnng m/z-> 20 25 30 35 40 45 50 55 60 65: 70 75 80 85 90 95 - 'Abundance #8865: DL-3.4-Dimethyl-3,4-hexanedioi A A I ' ' ' ' I ' ' 43 9.80 10.00 10.20 10.40 10.60 m/z 57.1.0 29.92% 5000 73 55 — . ........................ ’r•• •r•••r‘••l• . । , r, t r r। । ( , ( , । । , । ( । । । m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 9.80 10.00 10.20 10.40 10.60 J

LB.D NP112701.M Fri Dec 28 11:46:55 2001 Page 7

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