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GCMS analysis results for sample AD28164, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD28164 conducted on January 2, 2002.

NYC-WTC_000034562–000034578

Folder label: “GCMS X 11/23/01 A 12/21/01

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Scanned page image, NYC-WTC_000034577
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\LB.D Vial: 10 Acq On : 22 Dec 2001 2:07 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 10 Anthracene-dlO- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

25.08 20.00 ng/uL 4963960 Phenanthrene-dl0 25.22

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-d10- 188 C14D10 001719-06-8 96 2 Phenanthrene-d10 188 C14D10 001517-22-2 52 3 Antipyrine 188 C11H12N2O 000060-80-0 36 4 Selepd.de, ethyl 1-methyl-l-penten-3 188 C8H12Se m/z 188.20 100 .00% 33 025128-48-7 Abundance Scan 2207 (25.084 min): LB.D (-) 188

5000 - 80 ■ > l ■ • ■ • । 94 1 50 ill 24.80 25.00 25.20 25.40 42 52 66 . 1 92110118—132—148,—179 189 1— TT‘ m/z I"............ .................... 11 n.i | 80.05 17.35% mlz-? 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 ----- ' I1 ' 1 1 I ■ ■ 24.80 25.00 25.20 25.40

30 m/z 187.20 16.47% 66 94 160 I; I 1 '" I' 1* 'I'1 "I'' 1 1I'1 TI‘ TTTTTTTTTTTTTTT mH miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 188 / ( i r ■ ■ ■ 1 24.80 25.00 25.20 25.40 5000 m/z 94.15 16.36%

80 94 160 66 1 । 1 11 1 । 1 1 irpr TPTT i' ■'' i'''' i'''' i " 1' i'''' i V" rr r m/z-?........ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69176: Antipyrine 188 24.80 25.00 25.20 25.40 m/z189.20 14.72% 96 5000 77 56 105

HH +16 129 159 173 1 r "11" " i"'11" " r ■ ■ ■ i' i" " ।" " ।" ” । ■■" ।" " ।" " r1111111" i1 > ■ i • ■ • ■ । m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.80 25.00 25.20 25.40

LB.D NP112701.M Fri Dec 28 11:47:01 2001 Page 10

NYC-WTC_000034577

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NYC-WTC_000034577Source: NYC Law Department, mirrored locally

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