GCMS analysis results for sample AD28169, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28169.D Vial: 19 Acq On : 22 Dec 2001 11:14 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.08 20.00 ng/uL 6370300 Phenanthrene-dl0 25.22

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 96 V 2 Phenanthrene-d10 188 C14D10 001517-22-2 87 ) 3 Antipyrine V 4Benzene,_1-(1-cyclohexen-l-yl)-4-me 188 C13H160 188 C11H12N20 000060-80-0 36 020758-60-5 33 Abundance Scan 2207 (25.078 min)::281 69.D (-) m/z 188.20 100.00% 188

5000

80 94 160 42 52 66 , 24.80 25.00 25.20 25.40

miz-> 30 I’TTTTTTH 1102110,118.132 146+170,180— ‘I‘ m/z 80.05 17.55% 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 ■ ■ । ■ • ■ • i ■ ■ । • r• ■ ■ ■ । ■ 24.80 25.00 25.20 25.40 80 94 m/z 94.1,5 16.58% 66 160 mmmmm ■i"" r I n 111' miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-dW 188

24.80 25.00 25.20 25.40 5000 m/z 187.20 15.88%

66 80 94 160 i mmmmm m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69176: Antipyrine 188 24.80 25.00 25.20 25.40 m/z 189.20 14.60% 96 5000 77 56 105 i II 116T""IIITTT 129 159 173 ।■•■■।■■■■। ■ ........... TT‘‘‘‘T . 1 ’111011 ‘ IIT T i ■ ■ " I ■ ' ' i ■ ' ■ ' i -PPI miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.80 25.00 25.20 25.40

28169.D NP112701.M Fri Dec 28 09:59:40 2001 Page 3

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