GCMS analysis results for sample AD28169, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD28169 conducted on January 2, 2002.

NYC-WTC_000034706–000034717

Folder label: “GCMS X 11/23/01 A 12/21/01”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28169.D Vial: 19 Acq On : 22 Dec 2001 11:14 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Acenaphthene-diO Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

20.67 21.00 ng/uL 6690190 Phenanthrene-dl0 25.22

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acenaphthene-diO 164 C12D10 015067-26-2 93 2 Thiophene, 3-bromo- 162 C4H3BrS 000872-31-1 28 3 Thiophene, 2-bromo- 162 C4H3BrS 001003-09-4 28 4 Tricyc^Xo [4.4.0.02,7] dec-4-en-3-one, 162 C11H14O 006518-50-9 17 Abundance Scan 1726 (20.667 min): 28169.D (-) m/z 164.20 100.00% 64

5000 80 ,54 66 . 90 100 108 122 132 146 156 20.40 20.60 20.80 21.00 —311734 th H । H r I | I I I < | I M I 1111 I । ।।, I TIT ■ । ■ I I m/z 162.10 89.75% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #13561: Acen aphthene-d 10 162

/ 5000 20.40 20.60 20.80 21.00 80 m/z 160.10 40.51% 66 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 • M 132 _______ 11 ■ ■ ■ i ■'■ ■ i ■ L j__ ■11 ’ 1 I '1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #12744: Thiophene, 3-bramo- 164 ...................... /.......................... 83 20.40 20.60 20.80 21.00 5000 45 m/z 80.05 30.30%

57 ; 119 135 'I■''bl' "‘I''■.I' II—ur ' I TTur 11—————— TTTTT) ITT rp-rn-f. -m T m/z-> 30__ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #12743: Thiophene, 2-bromo- 162 20.40 20.60 20.80 21.00 m/z 163.20 17.87% 5000 83 45 i 38 58 i II 117 1______ _ , * I ‘ tt I ’ TT 1■ i ■ • ■' i • ■ ■ ■ i ■ ' ’ i *' ’' I • ''1 i ' •' 1 i'' ' ' i •'1' i''' • I • • I• • miz-2 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 20.40 20.60 20.80 21.00

28169.D NP112701.M Fri Dec 28 09:59:38 2001 Page 2

NYC-WTC_000034715

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