GCMS analysis results for sample AD28167, Jan 2002

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, Data File : C:\HPCHEM\l\DATA\DEC2101\28168.D vial: 18 Acq On : 22 Dec 2001 10:19 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Acenaphthene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

20.67 20.91 ng/uL 6599030 Phenanthrene-dl0 25.08

Hit# of Tentative ID MW MolForm CAS# Qual

1 Acenaphthene -diO 164 C12D10 015067-26-2 93 2 Thiophene, 2-bromo- 162 C4H3BrS 001003-09-4 28 3 T: cyclo[4.4.0.02,7]dec-4-en-3-one, 162 C11H140 006518-50-9 17 4 2-Benzothiazolamine, 6-methyl - 164 C8H8N2S _______ 002536-91-6 9 Abundance Scan 1726 (20.673 min): 28168.D (-) m/z 164.20 100.00% $4

5000 80 . FA 66 90 100 108 122 132 146 156 20.40 20.60 20.80 21.00 I mlz:—? ‘I" 30 —42144734 TTtmTT m/z 162.10 40__50 60 70_ 80 90 100 110 120 130 140 150 160 170 91.87% Abundance #13561: Acenaphthene-d10 162

5000 20.40 20.60 20.80 21.00 80 m/z 160.10 41.61% 66 mPPP 132 ■n , TTn‘puon—uuu‘T"OTTIII ‘T I_ ■ ■ I • <

miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #12743; Thiophene, 2-bromo- 162 20.40 20.60 20.80 21.00 5000- 83 m/z 80.15 28.33% 45 38 58 ‘I , , , rpTrrpnrrrpTTrpTrT|T> .................... ' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■................................... ■' • i ■ ■ ■ ■ i ■ ■ ■ ■ r ■ ■ ■ 11'11 ii1 i _ ; | ■ ■ i • • miz- 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #13004: Trtcyclo[4,4.0.02,7]dec-4-en-3-one, 6-methyl- ,......... 162 20.40 20.60 20.80 21.00 82 m/z 163.20 19.88% 5000 ... 119 134 ‘77 147 । I‘t‘III‘ZI1"TTIT, TTTTTT ......... "■'T 1.. li 1 TII* ■ ■ l ■ ■ ' ‘J"ITT TTTTEIITT miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 20.40 20.60 20.80 21.00

28168.D NP112701.M Fri Dec 28 09:59:13 2001 Page 10

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