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GCMS analysis results for sample AD27625, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD27625 conducted on January 3, 2002.

NYC-WTC_000033112–000033127

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033126
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27625.D Vial: 15 Acq On : 20 Dec 2001 10:39 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 Anthracene-dlO- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

25.17 20.00 ng/uL 7023600 Phenanthrene-dl0 25.31

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene- d10- 188 C14D10 001719-06-8 96 2 Phenanthr ,e-dl0 188 C14D10 001517-22-2 58 3 Benzene,/ 1-(1-cyclohexen-l-yl)-4-me 188 C13H160 020758-60-5 36 4 4-Fluoro-6-methyl-2-phenylpyrimidin 188 C11H9FN2 000000-00-0 36 'Abundance Scan 2217 (25.168 min): 27625.D (-) m/ z 188.20 100.00% 188

5000

। । । . । । । ( । ' I 1 ‘‘ • । • • • » । • 80 42 52 66 94 | 102110118 132 146 160 .i| 170 180, 24.80 25.00 25.20 25.40 25.60 r i i i |I II , I’H I I I I I I i TTTHTH TTTTTTmm TT m/z 187.20 17.78% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188

5000 - ...... A........ 24.80 25.00 25.20 25.40 25.60

80 94 m/z 80.05 17.12% 66 160 ,I T’ ' ' ' f ' ' ' ' I 1 TII‘ An I ’ ’ ’' I 4 i'11 ■ i' m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188 ................ , I । 24.80 25.00 25.20 25.40 25.60 5000- m/z 94.15 15.97%

80 94 160 |I ..... 66..... ..... ; i.............. ................... . I I......... ll m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19943: Benzene, 1-(1-cyclohexen-1-yl)-4-methoxy- 1 i f 1 1 ■ i ■ ' ' i 1 ' i ' • • ' I ' 188 24.80 25.00 25.20 25.40 25.60 m/z 189.20 14.86% 5000- 160

121129 145 173 _...... II..... - m/z-> 30 40 50 60 70 80 TP....4 90 100 110 120 130 140 150 160 170 180 190 ■' r 111 r ' 24.80 25.00 25.20 25.40 25.60

27625.D NP112701.M Thu Dec 20 11:40:35 2001 Page 7

NYC-WTC_000033126

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NYC-WTC_000033126Source: NYC Law Department, mirrored locally

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