GCMS analysis results for sample AD27549, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\27549.D Vial: 8 Acq On 13 Dec 2001 4:45 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 3-Methyl-l-[(1H)-1,2,4-triazol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

10.82 0.48 ng/uL 158801 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Methyl-1- 1H)-1,2,4-triazol-l-yl 153 C7H11N30> 064922-02-7 23 2 Cyclohexane/ azido- 125 C6H11N3 019573-22-9 12 3 Isoxazole/5-methyl- 83 C4H5NO 005765-44-6 9 4 1,4 -Pentadien-3-ol 84 C5H80 000922-65-6 9 Abundance Scan 652 (10.824 min): 27549.D (-) m/ z 43.10 100.00%l 43

83 5000 55 71 I > > > • ] ’ » ’ > । ■ rr 10.40 1060 10.80 11.00 11.20 Pge + I । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ '90 100110 120 130 140 150 160 m/ z 83 • 05 63.37% m/z-> 20 30 40 50 60 70 80 Abundance #10506: 3-Methyl-1-[(1H)-1,2,4-triazol-1-yl]butan-2-one 43 83

5000- 71 — 10.40 10.60 10.80 11.00 11.20 55 m/z 55.10 47.11% —IPPT ............. _ 154 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #4321: Cyclohexane, azido-

41 55 83 —A ' ■ i ' ' ' ' i ' ' 10.40 10.60 10.80 11.00 11.20 5000- m/z 71.05 35.54% 27 67 1 . 96 125 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance 43 #512: Isoxazole, 5-methyl- -A- ■ i > ■ ■ • i > ■ 10.40 10.60 10.80 11.00 11.20 m/z 58.10 27.96% 83 5000 68

27 54 TTTgr -i-pr-T-T-i-p- 1 ■' । ‘ ' i11111'' । ■ ■ ■ ■ । ■ ■ ■ ■ ।■11111111 1____ - 1 I ’ • ' ' 1 11 T.T ■ i ■ • miz- 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 10.40 10.60 10.80 11.00 11.20

27549.D NP112701.M Fri Dec 14 12:56:52 2001 Page 6

NYC-WTC_000033503