GCMS analysis results for sample AD28165, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD28165 conducted on January 2, 2002.

NYC-WTC_000034653–000034668

Folder label: “GCMS X 11/23/01 A 12/21/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\DEC21O1\281O6.D vial: 13 Acq On : 22 Dec 2001 4:51 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Cyclohexane, bromo- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.76 1.01 ng/uL 366116 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclohexane, bromo- 162 C6HllBr 000108-85-0 40 2 Cyc l ohexane , bromo - 162 C6HllBr 000108-85-0 40 3 Cyclohexane, bromo- 162 C6HllBr 000108-85-0 40 4 2-Hexene, 4,4,5-trimethyl- 126 C9H18 _______ 055702-61-9 33 Abundance Scan 646 (10.763 min): 28106.D (-) m/z 43.10 100.00% 43 83 55 5000 ----------- । -PFP 71

miz-> ■ i' ■ ■ ■ r 20 30 40 50 60 —— LL 11 ■ ■1 ■ i ■ + i ■ ■ ■ ■ r ' ■' r ■'' i ■'' ‘ i 70 80 90 100 110 120 130 140 150 160 170 I 10.40 10,60 10.80 11.00 11.20 m/z 83.15 81.42% Abundance #67631: Cyclohexane, bromo- 86

5000 55 10.40 10.60 10.80 11.00 11.20 m/z 55.10 67.16% 27 I ...... .67.....__ 11 ■'' ■ i'1'' i1' ■' i'' ■ ■ i ■ ■ ■' i' i ■ • > ■ I ■ ■ ■ ■ i''' ■ i 164 i1 ‘ ■ i ■ m/z-> 20 30 40 50 60 70 80 90 100 11 120 130 140 150 160 170 Abundance #67632. Cyclohexane, bromo- 83 -------.......................... 10.40 10.60 10.80 11.00 11.20 55 m/ 5000 41.10 28.45% 27 67 _______________________ 164 1111'' 11' ■' i " ■ ■ i IPmPTT I " ' ' I ' ' " I ■ ' ' ' r " ' I ' TI"T’’IIT Tn-rj-T m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #67630: Cyclohexane, bromo- "I • । • •• • । • 83 10.40 10.60 10.80 11.00 11.20 m/z 39.10 16.08% 55 1 5000

27 67 ।................................................ 162 mz-> TITTTITTTTTTT 20 30 40 50 60 70 +— Im80 90 100 110 120 130 140 150 160 170 ' ' i ' ■ ' ' i ' 10.40 10.60 10.80 11.00 11.20

28106.D NP112701.M Fri Dec 28 09:55:48 2001 Page 7

NYC-WTC_000034667

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NYC-WTC_000034667Source: NYC Law Department, mirrored locally

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NYC-WTC_000034579

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