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GCMS analysis results for sample AD27679, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27679 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033263–000033284

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033282
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC19 01\27679.D Vial: 6 Acq On 19 Dec 2001 11:43 am Operator: GALOS Sample gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *************************************************************** * * * * * * Peak Number 12 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

10.49 4.44 ng/uL 984282 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 36 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 32 3 Pentanal', 2,2-dimethyl- 114 C7H140 014250-88-5 25 4 Hydroxyl amine, O-hexyl- 117 C6H15NO 004665-68-3 25 Abundance Scan 616 (10.488 min): 27679.D (-) m/z 43.10 100.00% 43

5000-

57 85 1 1 i r 1 1 1 i J TTT A I7-

m/z-> i •1" r " ' i 20 25 30 l +5 39 61 69 -TPTTTTTTTTTTT 1—— 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 TTTT1 10.20 10.40 10.60 10.80 m/ Z 45.10 54.51% Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43 57 _ -j-T- 5000 71 85 i'-r 10.20 10.40 10.60 10.80 m/z 41.10 28.70% 100 mmp m Trp-rrrp-rTTY " I' ' ' ‘ I T1 1111 TTT V m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1773: 2-Pentanol, 4-methyl- 45 7 l.। A । । r । r i it । i'। .Ifn i ‘I " 10.20 10.40 10.60 10.80 5000 - m/ Z 85.15 21.09%

27 69 57 87 i I " " I' " ‘ I mm T’TTIIIITTTTTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #3038: Pentanal, 2,2-dimethyl- \ ■ •l*' ■■ l l < ■■ I ' ' TIPTT 43 10.20 10.40 10.60 10.80 m/z 57.10 15.44% 5000 - 85 27 39 57 72

m/z-> -rrp- .. ...... 4 I •' •' I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 I ■' ’ ’ I i'1 ■11 “ * • r'" i r ----- P -A- 10.20 10.40 10.60 10.80

27679.D NP112701.M Thu Dec 20 11:42:24 2001 Page 12

NYC-WTC_000033282

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