GCMS analysis results for sample AD27764, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27764.D Vial: 7 Acq On : 19 Dec 2001 12:38 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 15 Oxirane, 2-methyl-3-propyl-, e Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.49 3.96 ng/uL 1003550 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2-met 1-3-propyl-, cis- 100 C6H120 006124-90-9 36 2 3-Buten-2-ol •3-methyl- 86 C5H10O 010473-14-0 25 3 Pentanal, ,2-dimethyl- 114 C7H140 014250-88-5 25 4 Hexane., -propoxy­ 144 C9H20O 053685-78-2 23 Abundance Scan 616 (10.488 min): 27764.D (-) m/ z 43.10 100.00% 43

5000 85 — 57 i —

m/z-> — 147 39 + 1 61

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 69 100 TI’Tett TTT" m/z 10.20 10.40 10.60 10.80 45.05 42.37% Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43

5000 57 71 85 —4 A — — 10.20 10.40 10.60 10.80 m/ z 41.10 26.26% "I •'" I I ■ ■ r ■ ■ ■ i'' " i r"•i 100 i111' i'1111" •(i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #716: 3-Buten-2-ol. 3-methyl- 4b . . I i . TII I-1 TIT !■ -P 10.20 10.40 10.60 10.80 5000 39 ■ m/ z 85.15 23.43% 27 1 53 58 86 67 71 "i ■ ■ ■ •r TTT i" - ■ . । ■" * । r ' " r ' ■' i'" ' i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #3038: Pentanal, 2,2-dimethyl- k ■ ■ i ■ /1 ■ ■ ■ । 433 10.20 10.40 10.60 10.80 m/z 57.10 16.97% 5000 85 27 39 — 1111111111111 57 72 -— ------------ •r•‘•r • • i" • 'T‘ • • • i" " i • ‘111'1" l1 ”11 m/z-> 20 25 30 35 40 45 .50 55 60 65 70 75 80 85 90 95 100 105 10.20 10.40 10.60 10.80

27764.D NP112701.M Thu Dec 20 11:43:48 2001 Page 15

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